5-Iodonaphthalen-1-amine

Base Information

Chemical Name:5-Iodonaphthalen-1-amine
CAS No.:66640-75-3
Molecular Formula:C10H8IN
Molecular Weight:269.08169
Hs Code.:
DSSTox Substance ID:DTXSID20704750
Wikidata:Q82637278

Synonyms:5-iodonaphthalen-1-amine;66640-75-3;1-Amino- 5-iodonaphthalene;1-Amino-5-iodonaphthalene;SCHEMBL19070478;DTXSID20704750;CS-0312090;FT-0718482

Suppliers and Price of 5-Iodonaphthalen-1-amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Alichem
1-Amino-5-iodonaphthalene
1g
$ 1786.10

Alichem
1-Amino-5-iodonaphthalene
500mg
$ 1058.40

Alichem
1-Amino-5-iodonaphthalene
250mg
$ 714.00

Total 6 raw suppliers

Chemical Property of 5-Iodonaphthalen-1-amine

Chemical Property:

Melting Point:75 °C
Boiling Point:380.8±17.0 °C(Predicted)
PKA:3.45±0.10(Predicted)
PSA：26.02000
Density:1.819±0.06 g/cm3(Predicted)
LogP:3.60780
XLogP3:3.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:268.97015
Heavy Atom Count:12
Complexity:160

Purity/Quality:

97% ^*data from raw suppliers

1-Amino-5-iodonaphthalene ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC2=C(C=CC=C2I)C(=C1)N

Technology Process of 5-Iodonaphthalen-1-amine

There total 3 articles about 5-Iodonaphthalen-1-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 64567-10-8
1-Iodo-5-nitronaphthalene

: 66640-75-3
5-iodonaphthalene-1-amine

Guidance literature:: With tin(ll) chloride; In ethyl acetate; Heating;
DOI:10.1016/S0040-4039(03)00344-7

Reference yield:

: 3272-91-1
5-nitro-[1]naphthylamine

: 66640-75-3
5-iodonaphthalene-1-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / NaNO₂; KI; urea / H₂SO₄; acetic acid; H₂O / 0 °C

2: 93 percent / SnCl₂*2H₂O / ethyl acetate / 10 h / Heating

With urea; potassium iodide; tin(ll) chloride; sodium nitrite; In sulfuric acid; water; acetic acid; ethyl acetate;
DOI:10.1021/jo0203589

Reference yield:

: 605-71-0
1,5-dinitronaphthalene

: 66640-75-3
5-iodonaphthalene-1-amine

Guidance literature:: Multi-step reaction with 3 steps

1: 54 percent / NH₄Cl; 28percent aq. NH₃; Na₂S / H₂O / 4 h / 80 - 85 °C

2: 76 percent / NaNO₂; KI; urea / H₂SO₄; acetic acid; H₂O / 0 °C

3: 93 percent / SnCl₂*2H₂O / ethyl acetate / 10 h / Heating

With sodium sulfide; ammonium chloride; urea; potassium iodide; tin(ll) chloride; sodium nitrite; In sulfuric acid; water; acetic acid; ethyl acetate;
DOI:10.1021/jo0203589