ert-butyl 3-[3-(benzyloxy)phenyl]azetidine-1-carboxylate

Base Information

Chemical Name:ert-butyl 3-[3-(benzyloxy)phenyl]azetidine-1-carboxylate
CAS No.:916900-30-6
Molecular Formula:C21H25NO3
Molecular Weight:339.434
Hs Code.:2933990090
Mol file:916900-30-6.mol

Synonyms:ert-butyl 3-[3-(benzyloxy)phenyl]azetidine-1-carboxylate

Suppliers and Price of ert-butyl 3-[3-(benzyloxy)phenyl]azetidine-1-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
tert-Butyl3-(3-(benzyloxy)phenyl)azetidine-1-carboxylate 95+%
1g
$ 299.00

Chemenu
tert-butyl3-(3-(benzyloxy)phenyl)azetidine-1-carboxylate 95%
1g
$ 282.00

American Custom Chemicals Corporation
TERT-BUTYL-3-(3-(BENZYLOXY)PHENYL)AZETIDINE-1-CARBOXYLATE 95.00%
5MG
$ 495.56

Alichem
tert-Butyl3-(3-(benzyloxy)phenyl)azetidine-1-carboxylate
1g
$ 400.00

Total 9 raw suppliers

Chemical Property of ert-butyl 3-[3-(benzyloxy)phenyl]azetidine-1-carboxylate

Chemical Property:

PSA：38.77000
LogP:4.53780
Storage Temp.:2-8°C

Purity/Quality:

97% ^*data from raw suppliers

tert-Butyl3-(3-(benzyloxy)phenyl)azetidine-1-carboxylate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of ert-butyl 3-[3-(benzyloxy)phenyl]azetidine-1-carboxylate

There total 3 articles about ert-butyl 3-[3-(benzyloxy)phenyl]azetidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 107623-21-2
1-(benzyloxy)-3-iodobenzene

: 254454-54-1
tert-butyl-3-iodoazetidine-1-carboxylate

: 916900-30-6
tert-butyl 3-[3-(benzyloxy)phenyl]azetidine-1-carboxylate

Guidance literature:: tert-butyl-3-iodoazetidine-1-carboxylate; With chloro-trimethyl-silane; ethylene dibromide; zinc; In N,N-dimethyl-formamide; at 20 - 70 ℃; for 2.16667h;

1-(benzyloxy)-3-iodobenzene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; trifuran-2-yl-phosphane; In N,N-dimethyl-formamide; at 70 ℃; for 4h;

Reference yield:

: 916899-83-7
tert-butyl 3-{[(trifluoromethyl)sulfonyl]oxy}azetidine-1-carboxylate

: 916900-30-6
tert-butyl 3-[3-(benzyloxy)phenyl]azetidine-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium iodide / N,N-dimethyl-formamide / 18 h / 0 - 20 °C

2.1: chloro-trimethyl-silane; ethylene dibromide; zinc / N,N-dimethyl-formamide / 2.17 h / 20 - 70 °C

2.2: 4 h / 70 °C

With chloro-trimethyl-silane; ethylene dibromide; potassium iodide; zinc; In N,N-dimethyl-formamide;

Reference yield:

: 141699-55-0
tert-butyl 3-hydroxyazetidine-1-carboxylate

: 916900-30-6
tert-butyl 3-[3-(benzyloxy)phenyl]azetidine-1-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 2,6-dimethylpyridine / dichloromethane / 0.5 h / -30 °C

2.1: potassium iodide / N,N-dimethyl-formamide / 18 h / 0 - 20 °C

3.1: chloro-trimethyl-silane; ethylene dibromide; zinc / N,N-dimethyl-formamide / 2.17 h / 20 - 70 °C

3.2: 4 h / 70 °C

With 2,6-dimethylpyridine; chloro-trimethyl-silane; ethylene dibromide; potassium iodide; zinc; In dichloromethane; N,N-dimethyl-formamide;