5-Hydroxy-1-(4-hydroxy-3-methoxyphenyl)-3-tetradecanone

Base Information

Chemical Name:5-Hydroxy-1-(4-hydroxy-3-methoxyphenyl)-3-tetradecanone
CAS No.:107257-18-1
Molecular Formula:C21H34O4
Molecular Weight:350.499
Hs Code.:
Mol file:107257-18-1.mol

Synonyms:CAS号:107257-18-1分子式:C21H34O4分子量:350EINECS号:相关类别:Mol文件:107257-18-1.mol 5-羟基-1-(4-羟基-3-甲氧基苯基)-3-十四酮性质沸点500℃

Suppliers and Price of 5-Hydroxy-1-(4-hydroxy-3-methoxyphenyl)-3-tetradecanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 5-Hydroxy-1-(4-hydroxy-3-methoxyphenyl)-3-tetradecanone

Chemical Property:

Melting Point:40 °C (petroleum ether); 44 - 45 °C
Boiling Point:500℃
PKA:10.02±0.20(Predicted)
Flash Point:166℃
PSA：66.76000
Density:1.037
LogP:4.79420

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5-Hydroxy-1-(4-hydroxy-3-methoxyphenyl)-3-tetradecanone

There total 22 articles about 5-Hydroxy-1-(4-hydroxy-3-methoxyphenyl)-3-tetradecanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 112-31-2
caprinaldehyde

: 122-48-5
4-(4-hydroxy-3-methoxyphenyl)-2-butanone

: 107257-18-1
5-hydroxy-1-(4-hydroxy-3-methoxyphenyl)tetradecan-3-one

Guidance literature:: With n-butyllithium; lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 ℃; for 6h;
DOI:10.1080/00397919908086182

Reference yield: 78.0%

: 91815-22-4
4-{2-[2-(2-Hydroxy-undecyl)-[1,3]dioxolan-2-yl]-ethyl}-2-methoxy-phenol

: 107257-18-1
5-hydroxy-1-(4-hydroxy-3-methoxyphenyl)tetradecan-3-one

Guidance literature:: With hydrogen fluoride; In water; acetonitrile; for 0.5h; Ambient temperature;

Reference yield:

: 1080-12-2,22214-42-2
(E)-4-(4-hydroxy-3-methoxyphenyl)but-3-ene-2-one

: 107257-18-1
5-hydroxy-1-(4-hydroxy-3-methoxyphenyl)tetradecan-3-one

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / H₂ / Raney nickel / acetone

2: 84 percent / phenol, hexamethyldisilazane / benzene / Heating

3: 1.) lithium di-isopropylamide, 2.) 2M HCl / 1.) -78 deg C, 1 h, THF, 2.) ether

With hydrogenchloride; hydrogen; 1,1,1,3,3,3-hexamethyl-disilazane; lithium diisopropyl amide; phenol; nickel; In acetone; benzene;
DOI:10.1039/P19810000082