3-cyclopropyl-3-{[(9H-fluoren-9-ylmethoxy)carbonyl]amino}propanoic acid

Base Information

• Chemical Name: 3-cyclopropyl-3-{[(9H-fluoren-9-ylmethoxy)carbonyl]amino}propanoic acid
• CAS No.: 683217-51-8
• Molecular Formula: C₂₁H₂₁NO₄
• Molecular Weight: 351.402
• Mol file: 683217-51-8.mol

Synonyms:3-cyclopropyl-3-{[(9H-fluoren-9-ylmethoxy)carbonyl]amino}propanoic acid;FMOC-DL-3-AMINO-3-CYCLOPROPYL-PROPIONIC ACID

Chemical Property of 3-cyclopropyl-3-{[(9H-fluoren-9-ylmethoxy)carbonyl]amino}propanoic acid

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

3-CYCLOPROPYL-3-([(9H-FLUOREN-9-YLMETHOXY)CARBONYL]AMINO)PROPANOIC ACID 95.00% ^*data from reagent suppliers

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Technology Process of 3-cyclopropyl-3-{[(9H-fluoren-9-ylmethoxy)carbonyl]amino}propanoic acid

There total 2 articles about 3-cyclopropyl-3-{[(9H-fluoren-9-ylmethoxy)carbonyl]amino}propanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

(±)-(9H-fluoren-9-yl)methyl 3-cyclopropyl-5-oxoisoxazolidine-2-carboxylate → (±)-3-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-cyclopropylpropanoic acid (683217-51-8)

Guidance literature:

With acetic acid; zinc; In tetrahydrofuran; water; at 40 ℃; for 4h; chemoselective reaction; Inert atmosphere;

DOI:10.1002/ejoc.201700472

Reference yield:

N-(9-fluorenylmethoxycarbonyloxy)hydroxylamine (190656-01-0) → (±)-3-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-cyclopropylpropanoic acid (683217-51-8)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium 2,2-dimethyl-4-oxo-4H-1,3-dioxin-6-olate / ethyl acetate / 40 °C / Inert atmosphere

2: acetic acid; zinc / tetrahydrofuran; water / 4 h / 40 °C / Inert atmosphere

With acetic acid; sodium 2,2-dimethyl-4-oxo-4H-1,3-dioxin-6-olate; zinc; In tetrahydrofuran; water; ethyl acetate;

DOI:10.1002/ejoc.201700472

upstream raw materials:

N-(9-fluorenylmethoxycarbonyloxy)hydroxylamine

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