5-(1-methyl-1H-pyrazol-4-yl)-3-(1-(3-nitrobenzyl)-1H-pyrazol-4-yl)-1Hpyrrolo[2,3-b]pyridine

Base Information

Chemical Name:5-(1-methyl-1H-pyrazol-4-yl)-3-(1-(3-nitrobenzyl)-1H-pyrazol-4-yl)-1Hpyrrolo[2,3-b]pyridine
CAS No.:1450642-50-8
Molecular Formula:C₂₁H₁₇N₇O₂
Molecular Weight:399.412
Hs Code.:
Mol file:1450642-50-8.mol

Synonyms:5-(1-methyl-1H-pyrazol-4-yl)-3-(1-(3-nitrobenzyl)-1H-pyrazol-4-yl)-1Hpyrrolo[2,3-b]pyridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-(1-methyl-1H-pyrazol-4-yl)-3-(1-(3-nitrobenzyl)-1H-pyrazol-4-yl)-1Hpyrrolo[2,3-b]pyridine

Chemical Property:

Purity/Quality:: 98%min ^*data from raw suppliers

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Technology Process of 5-(1-methyl-1H-pyrazol-4-yl)-3-(1-(3-nitrobenzyl)-1H-pyrazol-4-yl)-1Hpyrrolo[2,3-b]pyridine

There total 9 articles about 5-(1-methyl-1H-pyrazol-4-yl)-3-(1-(3-nitrobenzyl)-1H-pyrazol-4-yl)-1Hpyrrolo[2,3-b]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1450643-07-8
C₂₈H₂₃N₇O₄S

: 1450642-50-8
5-(1-methyl-1H-pyrazol-4-yl)-3-(1-(3-nitrobenzyl)-1H-pyrazol-4-yl)-1H-pyrrolo[2,3-b]pyridine

Guidance literature:: With water; lithium hydroxide; In tetrahydrofuran; methanol; at 25 ℃; for 15h;
DOI:10.1016/j.bmcl.2013.06.071

Reference yield:

: 1450642-64-4
C₁₆H₂₀BN₃O₄

: 1450642-50-8
5-(1-methyl-1H-pyrazol-4-yl)-3-(1-(3-nitrobenzyl)-1H-pyrazol-4-yl)-1H-pyrrolo[2,3-b]pyridine

Guidance literature:: Multi-step reaction with 3 steps

1: sodium carbonate / toluene; ethanol; water / 2 h / 100 °C

2: sodium carbonate / toluene; ethanol; water / 12 h / 100 °C

3: lithium hydroxide; water / tetrahydrofuran; methanol / 15 h / 25 °C

With water; sodium carbonate; lithium hydroxide; In tetrahydrofuran; methanol; ethanol; water; toluene;
DOI:10.1016/j.bmcl.2013.06.071

Reference yield:

: 1450642-80-4
C₂₄H₁₈BrN₅O₄S

: 1450642-50-8
5-(1-methyl-1H-pyrazol-4-yl)-3-(1-(3-nitrobenzyl)-1H-pyrazol-4-yl)-1H-pyrrolo[2,3-b]pyridine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium carbonate / toluene; ethanol; water / 12 h / 100 °C

2: lithium hydroxide; water / tetrahydrofuran; methanol / 15 h / 25 °C

With water; sodium carbonate; lithium hydroxide; In tetrahydrofuran; methanol; ethanol; water; toluene;
DOI:10.1016/j.bmcl.2013.06.071