β-Ethoxyfuran-2-ethanol

Base Information

• Chemical Name: β-Ethoxyfuran-2-ethanol
• CAS No.: 14133-53-0
• Molecular Formula: C8H12O3
• Molecular Weight: 156.18
• Mol file: 14133-53-0.mol

Synonyms:β-Ethoxy-2-furanethanol;β-Ethoxyfuran-2-ethanol

Chemical Property of β-Ethoxyfuran-2-ethanol

Chemical Property:

• Boiling Point: 203.3±25.0 °C(Predicted)
• PKA: 14.12±0.10(Predicted)
• PSA: 42.60000
• Density: 1.094±0.06 g/cm3(Predicted)
• LogP: 1.34950

Purity/Quality:

b-ethoxy-2-Furanethanol 97.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of β-Ethoxyfuran-2-ethanol

There total 3 articles about β-Ethoxyfuran-2-ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

ethanol (64-17-5) + D-glucal (13265-84-4) → 2-(2-furyl)-2-ethoxyethanol (14133-53-0)

Guidance literature:

With indium triflate; In acetonitrile; for 3.5h; regioselective reaction;

DOI:10.1021/ol801917n

Reference yield: 25.0%

2-furyloxirane (2745-17-7) + ethanol (64-17-5) → 2-(2-furyl)-2-ethoxyethanol (14133-53-0)

Guidance literature:

for 18h; Ambient temperature;

DOI:10.1016/S0040-4020(01)81188-1

Reference yield:

→ 2-(2-furyl)-2-ethoxyethanol (14133-53-0)

Guidance literature:

beim Erhitzen von Tri-O-acetyl-D-glucal in 0.05N ethanol. H2SO4 auf 70grad, neben anderen Verb.;

upstream raw materials:

2-furyloxirane

ethanol

D-glucal

Refernces

• 1、 Mukherjee, Debaraj,Yousuf, Syed Khalid,Taneja, Subhash Chandra. "Domino transformation of D-glucal to racemic α-substituted α-hydroxy methyl furfuryl derivatives". supporting information; scheme or table. p. 4831 - 4834. Retrieved 2009/05/31.