1-Piperidinecarboxylic acid, 4-(methylphenylamino)-, 1,1-dimethylethyl ester

Base Information

Chemical Name:1-Piperidinecarboxylic acid, 4-(methylphenylamino)-, 1,1-dimethylethyl ester
CAS No.:904679-03-4
Molecular Formula:C₁₇H₂₆N₂O₂
Molecular Weight:290.406
Hs Code.:

Synonyms:1-Piperidinecarboxylic acid, 4-(methylphenylamino)-, 1,1-dimethylethyl ester

Suppliers and Price of 1-Piperidinecarboxylic acid, 4-(methylphenylamino)-, 1,1-dimethylethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 1-Piperidinecarboxylic acid, 4-(methylphenylamino)-, 1,1-dimethylethyl ester

Chemical Property:

Purity/Quality:: 99%, ^*data from raw suppliers

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Technology Process of 1-Piperidinecarboxylic acid, 4-(methylphenylamino)-, 1,1-dimethylethyl ester

There total 2 articles about 1-Piperidinecarboxylic acid, 4-(methylphenylamino)-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 125541-22-2
1-(tert-butoxycarbonyl)-4-phenylaminopiperidine

: 74-88-4
methyl iodide

: 904679-03-4
4-(methyl-phenyl-amino)-piperidine-1-carboxylic acid tert-butyl ester

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 7.5h;

Reference yield:

: 79099-07-3
N-tert-butyloxycarbonylpiperidin-4-one

: 62-53-3
aniline

: 904679-03-4
4-(methyl-phenyl-amino)-piperidine-1-carboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium tris(acetoxy)borohydride; acetic acid / 1,1-dichloroethane / 20 h / 20 °C

1.2: pH 10

2.1: potassium carbonate / N,N-dimethyl-formamide / 18 h / 20 °C

With sodium tris(acetoxy)borohydride; potassium carbonate; acetic acid; In 1,1-dichloroethane; N,N-dimethyl-formamide;