2,10-Phenanthrenediol, 4b,5,6,7,8,8a,9,10-octahydro-4b,8,8-trimethyl-1-(1-methylethyl)-, (4bS,8aS,10S)-

Base Information

Chemical Name:2,10-Phenanthrenediol, 4b,5,6,7,8,8a,9,10-octahydro-4b,8,8-trimethyl-1-(1-methylethyl)-, (4bS,8aS,10S)-
CAS No.:24338-19-0
Molecular Formula:C₂₀H₃₀O₂
Molecular Weight:302.457
Hs Code.:
Mol file:24338-19-0.mol

Synonyms:2,10-Phenanthrenediol, 4b,5,6,7,8,8a,9,10-octahydro-4b,8,8-trimethyl-1-(1-methylethyl)-, (4bS,8aS,10S)-;(4bS,8aS)-4b,5,6,7,8,8a,9,10-Octahydro-4b,8,8-trimethyl-1-isopropylphenanthrene-2,10α-diol;14-Isopropylpodocarpa-8,11,13-triene-7β,13-diol;7β-Hydroxytotarol;Totara-8,11,13-triene-7β,13-diol

Suppliers and Price of 2,10-Phenanthrenediol, 4b,5,6,7,8,8a,9,10-octahydro-4b,8,8-trimethyl-1-(1-methylethyl)-, (4bS,8aS,10S)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 2,10-Phenanthrenediol, 4b,5,6,7,8,8a,9,10-octahydro-4b,8,8-trimethyl-1-(1-methylethyl)-, (4bS,8aS,10S)-

Chemical Property:

Melting Point:200-201 °C(Solv: benzene (71-43-2); ligroine (8032-32-4))
Boiling Point:413.0±45.0 °C(Predicted)
PKA:10.75±0.70(Predicted)
PSA：40.46000
Density:1.054±0.06 g/cm3(Predicted)
LogP:5.03670

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,10-Phenanthrenediol, 4b,5,6,7,8,8a,9,10-octahydro-4b,8,8-trimethyl-1-(1-methylethyl)-, (4bS,8aS,10S)-

There total 3 articles about 2,10-Phenanthrenediol, 4b,5,6,7,8,8a,9,10-octahydro-4b,8,8-trimethyl-1-(1-methylethyl)-, (4bS,8aS,10S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1048-23-3
13-acetoxytotara-8,11,13-trien-7-one

: 24338-19-0
totara-8,11,13-triene-7β,13-diol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1016/S0968-0896(00)00096-1

Reference yield:

: 15340-82-6
13-acetoxytotara-8,11,13-triene

: 24338-19-0
totara-8,11,13-triene-7β,13-diol

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / NBS; CaCO₃ / tetrahydrofuran; H₂O / 1 h / 20 °C / Irradiation

2: 82 percent / LiAlH₄ / tetrahydrofuran / 2 h / 20 °C

With N-Bromosuccinimide; lithium aluminium tetrahydride; calcium carbonate; In tetrahydrofuran; water; 1: Oxidation / 2: Reduction;
DOI:10.1016/S0968-0896(00)00096-1