2-Phenanthrenol, 4b,5,6,7,8,8a,9,10-octahydro-4b,8,8-trimethyl-1-(1-methylethyl)-, acetate, (4bS,8aS)-

Base Information

• Chemical Name: 2-Phenanthrenol, 4b,5,6,7,8,8a,9,10-octahydro-4b,8,8-trimethyl-1-(1-methylethyl)-, acetate, (4bS,8aS)-
• CAS No.: 15340-82-6
• Molecular Formula: C₂₂H₃₂O₂
• Molecular Weight: 328.495
• Mol file: 15340-82-6.mol

Synonyms:2-Phenanthrenol,4b,5,6,7,8,8a,9,10-octahydro-4b,8,8-trimethyl-1-(1-methylethyl)-, acetate,(4bS,8aS)- (9CI); 2-Phenanthrenol,4b,5,6,7,8,8a,9,10-octahydro-4b,8,8-trimethyl-1-(1-methylethyl)-, acetate,(4bS-trans)-; Podocarpa-8,11,13-trien-13-ol, 14-isopropyl-, acetate (7CI,8CI);Totarol acetate; Totaryl acetate

Chemical Property of 2-Phenanthrenol, 4b,5,6,7,8,8a,9,10-octahydro-4b,8,8-trimethyl-1-(1-methylethyl)-, acetate, (4bS,8aS)-

Chemical Property:

• PSA: 26.30000
• LogP: 5.76550

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Phenanthrenol, 4b,5,6,7,8,8a,9,10-octahydro-4b,8,8-trimethyl-1-(1-methylethyl)-, acetate, (4bS,8aS)-

There total 1 articles about 2-Phenanthrenol, 4b,5,6,7,8,8a,9,10-octahydro-4b,8,8-trimethyl-1-(1-methylethyl)-, acetate, (4bS,8aS)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

trans-totarol (511-15-9) + acetic anhydride (108-24-7) → 13-acetoxytotara-8,11,13-triene (15340-82-6)

Guidance literature:

In pyridine; at 0 - 20 ℃; for 14h;

DOI:10.1016/S0968-0896(99)00162-5

Reference yield: 100.0%

13-acetoxytotara-8,11,13-triene (15340-82-6) → 13-acetoxytotara-8,11,13-trien-7-one (1048-23-3)

Guidance literature:

With chromium(VI) oxide; In acetic acid; for 72h; Ambient temperature;

DOI:10.1071/C96209

Reference yield: 44.0%

13-acetoxytotara-8,11,13-triene (15340-82-6) + lead(IV) tetraacetate (546-67-8) → 7α,13-diacetoxy-totara-8,11,13-triene (54146-29-1)

Guidance literature:

With acetic acid; at 100 ℃; for 4h;

DOI:10.1016/S0968-0896(00)00096-1

upstream raw materials:

trans-totarol

acetic anhydride

Downstream raw materials:

13-acetoxytotara-8,11,13-trien-7-one

7α,13-diacetoxy-totara-8,11,13-triene

7-oxototarol

totara-8,11,13-triene-7β,13-diol

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