4-BroMo-2-(trifluoroMethyl)acetophenone

Base Information

• Chemical Name: 4-BroMo-2-(trifluoroMethyl)acetophenone
• CAS No.: 1197231-94-9
• Molecular Formula: C₉H₆BrF₃O
• Molecular Weight: 267.045
• Hs Code.: 2914390090
• Mol file: 1197231-94-9.mol

Synonyms:4-BroMo-2-(trifluoroMethyl)acetophenone;1-[4-Bromo-2-(trifluoromethyl)phenyl]ethanone

Chemical Property of 4-BroMo-2-(trifluoroMethyl)acetophenone

Chemical Property:

• Boiling Point: 261.7±40.0 °C(Predicted)
• Density: 1.564±0.06 g/cm3(Predicted)

Purity/Quality:

97% ^*data from raw suppliers

1-[4-Bromo-2-(trifluoromethyl)phenyl]ethan-1-one ^*data from reagent suppliers

Safty Information:

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Technology Process of 4-BroMo-2-(trifluoroMethyl)acetophenone

There total 8 articles about 4-BroMo-2-(trifluoroMethyl)acetophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

dimethyl 2-(4-bromo-2-(trifluoromethyl)benzoyl)malonate → 1-(4-bromo-2-(trifluoromethyl)phenyl)ethan-1-one (1197231-94-9)

Guidance literature:

With bromobenzene; sulfuric acid; at 120 - 130 ℃; for 2h; Temperature;

Reference yield: 82.0%

4-bromo-N-methoxy-N-methyl-2-(trifluoromethyl)benzamide + methylmagnesium bromide (75-16-1) → 1-(4-bromo-2-(trifluoromethyl)phenyl)ethan-1-one (1197231-94-9)

Guidance literature:

In tetrahydrofuran; at 0 ℃; for 5h;

Reference yield:

4-bromo-1-iodo-2-(trifluoromethyl)benzene (364-12-5) + tributyl(1-ethoxyvinyl)stannane (97674-02-7) → 1-(4-bromo-2-(trifluoromethyl)phenyl)ethan-1-one (1197231-94-9)

Guidance literature:

With dichlorobis(triphenylphosphine)palladium(II); In toluene; at 100 ℃; for 0.5h;

upstream raw materials:

4-bromo-2-(trifluoromethyl)benzoic acid

methylmagnesium bromide

4-bromo-1-iodo-2-(trifluoromethyl)benzene

tributyl(1-ethoxyvinyl)stannane

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