4-CYANO-ALPHA-CHLORO BENZALDOXIME

Base Information

• Chemical Name: 4-CYANO-ALPHA-CHLORO BENZALDOXIME
• CAS No.: 123476-70-0
• Molecular Formula: C8H5ClN2O
• Molecular Weight: 180.593
• Mol file: 123476-70-0.mol

Synonyms:4-CYANO-ALPHA-CHLORO BENZALDOXIME

Chemical Property of 4-CYANO-ALPHA-CHLORO BENZALDOXIME

Chemical Property:

• PSA: 56.38000
• LogP: 1.93288

Purity/Quality:

4-CYANO-ALPHA-CHLOROBENZALDOXIME 95 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-CYANO-ALPHA-CHLORO BENZALDOXIME

There total 7 articles about 4-CYANO-ALPHA-CHLORO BENZALDOXIME which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

4-cyanobenzaldehyde oxime (52707-54-7,52707-59-2,64847-77-4) → 4-cyano-N-hydroxy-benzenecarboximidoyl chloride (123476-70-0)

Guidance literature:

With N-chloro-succinimide; In N,N-dimethyl-formamide; at 25 ℃;

DOI:10.1021/jm0612867

Reference yield: 93.0%

4-cyanobenzaldehyde oxime (52707-54-7,52707-59-2,64847-77-4) → (Z)-4-cyano-N-hydroxybenzimidoyl chloride (123476-70-0)

Guidance literature:

With N-chloro-succinimide; In N,N-dimethyl-formamide; for 3h;

DOI:10.1021/jm960626t

Reference yield:

(E)-4-((hydroxyamino)methyl)benzonitrile (52707-54-7) → (Z)-4-cyano-N-hydroxybenzimidoyl chloride (123476-70-0)

Guidance literature:

With N-chloro-succinimide; In N,N-dimethyl-formamide; at 20 ℃; for 20h;

upstream raw materials:

4-cyanobenzaldehyde oxime

(E)-4-((hydroxyamino)methyl)benzonitrile

4-cyanobenzaldehyde

Downstream raw materials:

3-(p-cyanophenyl)-2-isoxazoline

4-(5-Oxo-4-phenyl-4,5-dihydro-isoxazol-3-yl)-benzonitrile

[3-(4-Cyano-phenyl)-4,5-dihydro-isoxazol-5-yl]-acetic acid methyl ester

4-cyano-benzonitrile N-oxide

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