1-(2-azidoethyl)azepane

Base Information

Chemical Name:1-(2-azidoethyl)azepane
CAS No.:1175146-65-2
Molecular Formula:C₈H₁₆N₄
Molecular Weight:168.242
Hs Code.:
Mol file:1175146-65-2.mol

Synonyms:1-(2-azidoethyl)azepane

Suppliers and Price of 1-(2-azidoethyl)azepane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 1-(2-azidoethyl)azepane

Chemical Property:

PSA：52.99000
LogP:1.56336

Purity/Quality:: ≥95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-(2-azidoethyl)azepane

There total 5 articles about 1-(2-azidoethyl)azepane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 26487-67-2
1-(2-chloroethyl)azepane hydrochloride

: 1175146-65-2
1-(2-azidoethyl)azepane

Guidance literature:: With sodium azide; In water; at 80 ℃;
DOI:10.1002/pola.27048

Reference yield:

: 51388-00-2
2-azepan-1-ylethylamine

: 1175146-65-2
1-(2-azidoethyl)azepane

Guidance literature:: With copper(ll) sulfate pentahydrate; triflic azide; potassium carbonate; In ethanol; water; toluene; at 20 ℃;
DOI:10.1021/acschemneuro.5b00058

Reference yield:

: 111-49-9
hexamethylene imine

: 1175146-65-2
1-(2-azidoethyl)azepane

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / ethanol / Reflux

2: hydrazine hydrate / ethanol / 0.75 h / Reflux

3: triflic azide; potassium carbonate; copper(ll) sulfate pentahydrate / ethanol; water; toluene / 20 °C

With copper(ll) sulfate pentahydrate; triflic azide; potassium carbonate; hydrazine hydrate; triethylamine; In ethanol; water; toluene;
DOI:10.1021/acschemneuro.5b00058