2-(diphenylphosphino)-N-(pyridin-2-ylMethyl)ethanaMine

Base Information

Chemical Name:2-(diphenylphosphino)-N-(pyridin-2-ylMethyl)ethanaMine
CAS No.:1388712-98-8
Molecular Formula:C20H21N2P
Molecular Weight:320.374
Hs Code.:
Mol file:1388712-98-8.mol

Synonyms:2-(diphenylphosphino)-N-(pyridin-2-ylMethyl)ethanaMine;N-[2-(Diphenylphosphino)ethyl]-2-pyridinemethanamine

Suppliers and Price of 2-(diphenylphosphino)-N-(pyridin-2-ylMethyl)ethanaMine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 2-(diphenylphosphino)-N-(pyridin-2-ylMethyl)ethanaMine

Chemical Property:

PSA：38.51000
LogP:3.69500

Purity/Quality:: 98%,99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-(diphenylphosphino)-N-(pyridin-2-ylMethyl)ethanaMine

There total 5 articles about 2-(diphenylphosphino)-N-(pyridin-2-ylMethyl)ethanaMine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1388712-97-7
PyCH=NCH₂CH₂PPh₂

: 1388712-98-8
2-(diphenylphosphaneyl)-N-(pyridin-2-ylmethyl)ethan-1-amine

Guidance literature:: With methanol; sodium tetrahydroborate; for 2.5h; Inert atmosphere;

Reference yield: 86.0%

: 1121-60-4
pyridine-2-carbaldehyde

: 4848-43-5
(2-aminoethyl)diphenylphosphane

: 1388712-98-8
2-(diphenylphosphaneyl)-N-(pyridin-2-ylmethyl)ethan-1-amine

Guidance literature:: pyridine-2-carbaldehyde; (2-aminoethyl)diphenylphosphane; With diisobutylaluminium hydride; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;

With diisobutylaluminium hydride; In tetrahydrofuran; toluene; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1002/anie.201805630

Reference yield:

: 4848-43-5
(2-aminoethyl)diphenylphosphane

: 1388712-98-8
2-(diphenylphosphaneyl)-N-(pyridin-2-ylmethyl)ethan-1-amine

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 3 h / 20 °C / Schlenk technique; Glovebox; Inert atmosphere

2: sodium tetrahydroborate; methanol / 2 h / Schlenk technique; Glovebox; Inert atmosphere

With methanol; sodium tetrahydroborate; In tetrahydrofuran;