2-amino-2-methyl-6-Heptenoic acid

Base Information

• Chemical Name: 2-amino-2-methyl-6-Heptenoic acid
• CAS No.: 1824552-06-8
• Molecular Weight: 157.21
• Mol file: 1824552-06-8.mol

Synonyms:2-amino-2-methyl-6-Heptenoic acid;6-Heptenoic acid, 2-amino-2-methyl-

Chemical Property of 2-amino-2-methyl-6-Heptenoic acid

Chemical Property:

Purity/Quality:

99.0%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-amino-2-methyl-6-Heptenoic acid

There total 14 articles about 2-amino-2-methyl-6-Heptenoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

(-)-(3S,5R)-3-methyl-3-(pent-4-enyl)-5-phenylmorpholin-2-one (1379761-96-2) → (+)-(S)-2-amino-2-methylhept-6-enoic acid (1011309-61-7,1824552-06-8)

Guidance literature:

(-)-(3S,5R)-3-methyl-3-(pent-4-enyl)-5-phenylmorpholin-2-one; With lithium hydroxide monohydrate; water; In tetrahydrofuran; for 3h; Inert atmosphere;

With methanol; water; lead(IV) tetraacetate; In dichloromethane; at 0 ℃; for 5h; Inert atmosphere;

DOI:10.1002/chem.201102351

Reference yield: 80.0%

C33H35N3NiO3 → (+)-(S)-2-amino-2-methylhept-6-enoic acid (1011309-61-7,1824552-06-8)

Guidance literature:

With hydrogenchloride; In methanol; at 65 ℃; for 3h;

DOI:10.1016/j.tet.2019.130485

Reference yield: 78.0%

C33H35N3NiO3 → (R)-2-amino-2-methylhept-6-enoic acid (1824552-06-8)

Guidance literature:

With hydrogenchloride; In methanol; at 65 ℃; for 3h;

DOI:10.1016/j.tet.2019.130485

upstream raw materials:

2-amino-2-methyl-6-heptenoic acid amide

hept-6-en-2-one

2-acetyl-hex-5-enoic acid methyl ester

(R)-3-(pent-4-enyl)-5-phenyl-5,6-dihydro-2H-1,4-oxazin-2-one

Downstream raw materials:

(S)-2-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-2-methylhept-6-enoic acid

(R)-2-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-2-methylhept-6-enoic acid