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α,α-Dibromo-o-tolunitrile

Base Information Edit
  • Chemical Name:α,α-Dibromo-o-tolunitrile
  • CAS No.:655-63-0
  • Molecular Formula:C8H5Br2N
  • Molecular Weight:274.942
  • Hs Code.:
  • Mol file:655-63-0.mol
α,α-Dibromo-o-tolunitrile

Synonyms:2-(Dibromomethyl)benzonitrile;o-Cyanobenzal bromide;o-Cyanobezylidene bromide;α,α-Dibromo-o-tolunitrile

Suppliers and Price of α,α-Dibromo-o-tolunitrile
Supply Marketing:Edit
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
Manufacturers and distributors:
  • Manufacture/Brand
  • Chemicals and raw materials
  • Packaging
  • price
  • TRC
  • 2-Dibromomethyl-benzonitrile
  • 500mg
  • $ 450.00
  • American Custom Chemicals Corporation
  • 2-DIBROMOMETHYL-BENZONITRILE 95.00%
  • 5MG
  • $ 501.70
Total 12 raw suppliers
Chemical Property of α,α-Dibromo-o-tolunitrile Edit
Chemical Property:
  • PSA:23.79000 
  • LogP:3.34668 
  • Storage Temp.:Hygroscopic, Refrigerator, under inert atmosphere 
  • Solubility.:Chloroform (Slightly), Methanol (Slightly) 
Purity/Quality:

> 95% *data from raw suppliers

2-Dibromomethyl-benzonitrile *data from reagent suppliers

Safty Information:
  • Pictogram(s):  
  • Hazard Codes: 
MSDS Files:

SDS file from LookChem

Useful:
  • Uses 2-Dibromomethyl-benzonitrile is an impurity of Alogliptin (A575425), which is an oral antihyperglycemic agent that is a selective inhibitor of the enzyme dipeptidyl peptidase-4 (DPP-4).Antidiabetic agent.
Technology Process of α,α-Dibromo-o-tolunitrile

There total 2 articles about α,α-Dibromo-o-tolunitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With N-Bromosuccinimide; dibenzoyl peroxide; In tetrachloromethane; at 85 ℃; for 24h;
DOI:10.1021/jo801219j
Guidance literature:
at 150 - 200 ℃; bei der Bromierung im Sonnenlicht;
Guidance literature:
With water; silver nitrate; In acetonitrile; for 0.333333h; Reflux;
DOI:10.1021/jo801219j
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