DL-MANDELIC ACID ISOAMYL ESTER

Base Information

Chemical Name:DL-MANDELIC ACID ISOAMYL ESTER
CAS No.:95360-05-7
Molecular Formula:C₁₃H₁₈O₃
Molecular Weight:222.284
Hs Code.:
Mol file:95360-05-7.mol

Synonyms:ISOAMYL DL-MANDELATE;ISOPENTYL DL-MANDELATE;DL-MANDELIC ACID ISOPENTYL ESTER;DL-MANDELIC ACID ISOAMYL ESTER

Suppliers and Price of DL-MANDELIC ACID ISOAMYL ESTER

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of DL-MANDELIC ACID ISOAMYL ESTER

Chemical Property:

PSA：46.53000
LogP:2.30930

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s): Xi
Hazard Codes:Xi
Statements: 38
Safety Statements: 26-36

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of DL-MANDELIC ACID ISOAMYL ESTER

There total 6 articles about DL-MANDELIC ACID ISOAMYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 123-51-3
i-Amyl alcohol

: 20698-91-3
(R)-methyl mandelate

: 1253176-72-5,95360-05-7
(R)-α-hydroxyphenylacetic acid iso-amyl ester

Guidance literature:: With scandium trifluoromethanesulfonate; Inert atmosphere; Reflux;
DOI:10.1002/ejoc.201701400

Reference yield: 61.0%

: isopentyl 2-diazo-2-phenylacetate

: 5421-04-5,95360-05-7
isopentyl 2-hydroxy-2-phenylacetate

Guidance literature:: With C₁₈BF₁₅*(x)H₂O; water; at 40 ℃; for 5h; Sealed tube; Schlenk technique;
DOI:10.1021/acs.orglett.8b01988

Reference yield: 40.0%

: 5421-04-5,95360-05-7
isopentyl 2-hydroxy-2-phenylacetate

: 1253176-72-5,95360-05-7
(R)-α-hydroxyphenylacetic acid iso-amyl ester

: 31221-84-8
iso-pentyl 2-oxo-2-phenylacetate

Guidance literature:: With 2,2,6,6-tetramethyl-piperidine-N-oxyl; N,N’-bis(salicylidene)-1,1’-binaphthyl-2,2’-diamine; oxygen; cobalt(II) diacetate tetrahydrate; In toluene; at 90 ℃; for 7h; under 760.051 Torr; optical yield given as %ee; enantioselective reaction;
DOI:10.1039/c0cc01917h