2,2,2-Trifluoro-1-phenyl-ethanone O-[(4-Methylphenyl)sulfonyl]oxiMe

Base Information

Chemical Name:2,2,2-Trifluoro-1-phenyl-ethanone O-[(4-Methylphenyl)sulfonyl]oxiMe
CAS No.:40618-87-9
Molecular Formula:C15H12F3NO3S
Molecular Weight:343.326
Hs Code.:
Mol file:40618-87-9.mol

Synonyms:2,2,2-Trifluoro-1-phenyl-ethanone O-[(4-Methylphenyl)sulfonyl]oxiMe

Suppliers and Price of 2,2,2-Trifluoro-1-phenyl-ethanone O-[(4-Methylphenyl)sulfonyl]oxiMe

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2,2,2-Trifluoro-1-phenyl-ethanoneO-[(4-Methylphenyl)sulfonyl]oxime
1g
$ 1320.00

Medical Isotopes, Inc.
2,2,2-Trifluoro-1-phenyl-ethanoneO-[(4-Methylphenyl)sulfonyl]oxime
100 mg
$ 650.00

American Custom Chemicals Corporation
2,2,2-TRIFLUORO-1-PHENYL-ETHANONE O-[(4-METHYLPHENYL)SULFONYL]OXIME 95.00%
5MG
$ 496.11

Total 3 raw suppliers

Chemical Property of 2,2,2-Trifluoro-1-phenyl-ethanone O-[(4-Methylphenyl)sulfonyl]oxiMe

Chemical Property:

PSA：64.11000
LogP:4.74770
Solubility.:Dichloromethane, Diethy Ether, Ethyl Acetate

Purity/Quality:

99% ^*data from raw suppliers

2,2,2-Trifluoro-1-phenyl-ethanoneO-[(4-Methylphenyl)sulfonyl]oxime ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses 2,2,2-Trifluoro-1-phenyl-ethanone O-[(4-Methylphenyl)sulfonyl]oxime is an intermediate in the synthesis of a diazirine photophore useful in photoaffinity labelling.

Technology Process of 2,2,2-Trifluoro-1-phenyl-ethanone O-[(4-Methylphenyl)sulfonyl]oxiMe

There total 4 articles about 2,2,2-Trifluoro-1-phenyl-ethanone O-[(4-Methylphenyl)sulfonyl]oxiMe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 655-25-4
2,2,2-trifluoroacetophenone oxime

: 98-59-9
p-toluenesulfonyl chloride

: 40618-87-9
C₁₅H₁₂F₃NO₃S

Guidance literature:: 2,2,2-trifluoroacetophenone oxime; With triethylamine; In acetone; at 0 ℃; for 0.25h;

p-toluenesulfonyl chloride; In acetone; for 3h; Reagent/catalyst; Temperature;

Reference yield:

: 434-45-7
2,2,2-Trifluoroacetophenone

: 40618-87-9
C₁₅H₁₂F₃NO₃S

Guidance literature:: Multi-step reaction with 2 steps

1: hydroxylamine hydrochloride; pyridine / 1 h / 70 °C

2: triethylamine / acetone / 1 h / 0 - 20 °C

With pyridine; hydroxylamine hydrochloride; triethylamine; In acetone;
DOI:10.1021/ol503630z

Reference yield:

: C₂₀H₂₂F₃N₃O₂S

: 40618-87-9
C₁₅H₁₂F₃NO₃S

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen iodide / acetonitrile / 1 h / 20 °C

2: hydroxylamine hydrochloride; pyridine / 7 h / 70 °C

3: triethylamine / acetone / 3 h / 0 - 20 °C

With pyridine; hydroxylamine hydrochloride; hydrogen iodide; triethylamine; In acetone; acetonitrile;
DOI:10.1021/jacs.0c09403