4-Methyl-N-(5-oxo-5,6,7,8-tetrahydronaphthalen-2-yl)benzenesulfonaMide

Base Information

• Chemical Name: 4-Methyl-N-(5-oxo-5,6,7,8-tetrahydronaphthalen-2-yl)benzenesulfonaMide
• CAS No.: 16204-16-3
• Molecular Formula: C17H17NO3S
• Molecular Weight: 315.38678
• Hs Code.: 2935009090
• Mol file: 16204-16-3.mol

Synonyms:4-Methyl-N-(5-oxo-5,6,7,8-tetrahydronaphthalen-2-yl)benzenesulfonaMide

Chemical Property of 4-Methyl-N-(5-oxo-5,6,7,8-tetrahydronaphthalen-2-yl)benzenesulfonaMide

Chemical Property:

• Melting Point: 216-222 °C
• Boiling Point: 505.0±60.0 °C(Predicted)
• PKA: 7.24±0.20(Predicted)
• PSA: 71.62000
• Density: 1.324±0.06 g/cm3(Predicted)
• LogP: 4.46860

Purity/Quality:

98%min ^*data from raw suppliers

4-Methyl-N-(5-oxo-5,6,7,8-tetrahydronaphthalen-2-yl)benzenesulfonamide 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-Methyl-N-(5-oxo-5,6,7,8-tetrahydronaphthalen-2-yl)benzenesulfonaMide

There total 2 articles about 4-Methyl-N-(5-oxo-5,6,7,8-tetrahydronaphthalen-2-yl)benzenesulfonaMide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

6-amino-1-tetralone (3470-53-9) + p-toluenesulfonyl chloride (98-59-9) → 4-Methyl-N-(5-oxo-5,6,7,8-tetrahydro-naphthalen-2-yl)-benzenesulfonamide (16204-16-3)

Guidance literature:

With pyridine; for 16h; Reflux;

DOI:10.5935/0103-5053.20160065

Reference yield:

→ 4-Methyl-N-(5-oxo-5,6,7,8-tetrahydro-naphthalen-2-yl)-benzenesulfonamide (16204-16-3)

Guidance literature:

/BRN= 207358/, TosCl;

Reference yield:

4-Methyl-N-(5-oxo-5,6,7,8-tetrahydro-naphthalen-2-yl)-benzenesulfonamide (16204-16-3) → N-(5-hydroxy-5,6,7,8-tetrahydronaphthalen-2-yl)-4-methylbenzenesulfonamide

Guidance literature:

With sodium tetrahydroborate; In methanol; at 0 - 20 ℃; for 1h;

DOI:10.5935/0103-5053.20160065

upstream raw materials:

6-amino-1-tetralone

p-toluenesulfonyl chloride

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