3-Methoxy-3'-nitro-1,1'-biphenyl

Base Information

Chemical Name:3-Methoxy-3'-nitro-1,1'-biphenyl
CAS No.:128923-93-3
Molecular Formula:C₁₃H₁₁NO₃
Molecular Weight:229.235
Hs Code.:2909309090
DSSTox Substance ID:DTXSID00563968
Wikidata:Q82448525
Mol file:128923-93-3.mol

Synonyms:3-Methoxy-3'-nitro-1,1'-biphenyl;128923-93-3;1-(3-Methoxyphenyl)-3-nitrobenzene;3'-METHOXY-3-NITROBIPHENYL;SCHEMBL20557970;DTXSID00563968;MFCD09909440;AKOS015999017;1,1'-Biphenyl, 3-methoxy-3'-nitro-;BS-20630;A888946

Suppliers and Price of 3-Methoxy-3'-nitro-1,1'-biphenyl

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
3-Methoxy-3''-nitro-1,1''-biphenyl
100mg
$ 60.00

TRC
3-Methoxy-3''-nitro-1,1''-biphenyl
50mg
$ 45.00

Crysdot
3-Methoxy-3'-nitro-1,1'-biphenyl 95+%
5g
$ 339.00

Crysdot
3-Methoxy-3'-nitro-1,1'-biphenyl 95+%
10g
$ 564.00

American Custom Chemicals Corporation
3-METHOXY-3'-NITRO-1,1'-BIPHENYL 95.00%
5MG
$ 500.97

Alichem
3-Methoxy-3'-nitro-1,1'-biphenyl
5g
$ 400.00

AK Scientific
1-(3-Methoxyphenyl)-3-nitrobenzene
10g
$ 851.00

AK Scientific
1-(3-Methoxyphenyl)-3-nitrobenzene
5g
$ 531.00

AK Scientific
1-(3-Methoxyphenyl)-3-nitrobenzene
1g
$ 211.00

Total 7 raw suppliers

Chemical Property of 3-Methoxy-3'-nitro-1,1'-biphenyl

Chemical Property:

PSA：55.05000
LogP:3.79360
Storage Temp.:2-8°C
XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:229.07389321
Heavy Atom Count:17
Complexity:264

Purity/Quality:

97% ^*data from raw suppliers

3-Methoxy-3''-nitro-1,1''-biphenyl ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=CC(=C1)C2=CC(=CC=C2)[N+](=O)[O-]

Technology Process of 3-Methoxy-3'-nitro-1,1'-biphenyl

There total 9 articles about 3-Methoxy-3'-nitro-1,1'-biphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 645-00-1
m-iodonitrobenzene

: 10365-98-7,1107579-37-2
3-methoxyphenylboronic acid

: 128923-93-3
1‐(3‐methoxyphenyl)‐3‐nitrobenzene

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In ethanol; toluene; for 2h; Heating;
DOI:10.1021/jm031140x

Reference yield: 92.0%

: 10365-98-7,1107579-37-2
3-methoxyphenylboronic acid

: 80858-83-9
3-nitrophenoxysulfonyl fluoride

: 128923-93-3
1‐(3‐methoxyphenyl)‐3‐nitrobenzene

Guidance literature:: With palladium diacetate; triethylamine; In ethanol; water; at 25 ℃; for 10h;
DOI:10.1039/d0ob00406e

Reference yield: 81.0%

: 2845-89-8
1-chloro-3-methoxy-benzene

: 585-79-5
m-nitrobromobenzene

: 128923-93-3
1‐(3‐methoxyphenyl)‐3‐nitrobenzene

Guidance literature:: m-nitrobromobenzene; With (2-(anthracen-9-yl)-1H-inden-3-yl)dicyclohexylphosphine; potassium acetate; bis(pinacol)diborane; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In N,N-dimethyl acetamide; at 100 ℃; for 3h; Inert atmosphere; Schlenk technique;

1-chloro-3-methoxy-benzene; With potassium phosphate tribasic trihydrate; In N,N-dimethyl acetamide; at 100 ℃; for 16h; Inert atmosphere; Schlenk technique;
DOI:10.1039/c4ob02436b