3-nitrophenoxysulfonyl fluoride

Base Information

• Chemical Name: 3-nitrophenoxysulfonyl fluoride
• CAS No.: 80858-83-9
• Molecular Formula: C₆H₄FNO₅S
• Molecular Weight: 221.166
• Mol file: 80858-83-9.mol

Synonyms:3-nitrophenoxysulfonyl fluoride

Chemical Property of 3-nitrophenoxysulfonyl fluoride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-nitrophenoxysulfonyl fluoride

There total 3 articles about 3-nitrophenoxysulfonyl fluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

meta-nitrophenol (554-84-7) → 3-nitrophenoxysulfonyl fluoride (80858-83-9)

Guidance literature:

With fluorosulfonyl fluoride; triethylamine; In dichloromethane; at 20 ℃; Sealed tube;

DOI:10.1002/anie.202007211

Reference yield: 10.0%

nitrobenzene (98-95-3,26969-40-4) → 4-nitrophenyl sulfurofluoridate (51451-34-4) + 2-nitrophenyl sulfurofluoridate (80858-87-3) + 3-nitrophenoxysulfonyl fluoride (80858-83-9)

Guidance literature:

With bis(fluorosulfuryl) peroxide; In 1,1,2-Trichloro-1,2,2-trifluoroethane; 1.) -30 deg C, 2 h, 2.) 20 deg C, 1 d;

DOI:10.1007/BF01094662

Reference yield:

→ 3-nitrophenoxysulfonyl fluoride (80858-83-9)

Guidance literature:

upstream raw materials:

nitrobenzene

meta-nitrophenol

Downstream raw materials:

3-nitro-1,1'-biphenyl

1‐(3‐methoxyphenyl)‐3‐nitrobenzene