Methyl 6-iodonicotinate

Base Information

Chemical Name:Methyl 6-iodonicotinate
CAS No.:173157-33-0
Molecular Formula:C7H6INO2
Molecular Weight:263.035
Hs Code.:2933399090
European Community (EC) Number:958-893-6
DSSTox Substance ID:DTXSID30563976
Nikkaji Number:J2.742.152K
Wikidata:Q82448537
Mol file:173157-33-0.mol

Synonyms:Methyl 6-iodonicotinate;173157-33-0;methyl 6-iodopyridine-3-carboxylate;Methyl6-Iodonicotinate;3-Pyridinecarboxylic acid, 6-iodo-, methyl ester;MFCD12546492;6-Iodo-nicotinic Acid Methyl Ester;SCHEMBL4918065;DTXSID30563976;CGFVEUUNDFAFHE-UHFFFAOYSA-N;YGA15733;methyl 6-iodo-pyridine-3-carboxylate;AKOS015853885;GS-5001;SY026656;CS-0150768;EN300-3221765;A881807

Suppliers and Price of Methyl 6-iodonicotinate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
Methyl6-iodonicotinate 95+%
5g
$ 461.00

Chemenu
Methyl6-iodonicotinate 95%
5g
$ 431.00

Chemcia Scientific
6-Iodo-nicotinicacidmethylester ＞95%
5 G
$ 350.00

American Custom Chemicals Corporation
METHYL-6-IODONICOTINATE 95.00%
5MG
$ 500.59

Alichem
Methyl6-iodonicotinate
5g
$ 387.92

AK Scientific
Methyl6-iodonicotinate
10g
$ 1217.00

AK Scientific
Methyl6-iodonicotinate
1g
$ 237.00

Aaron Chemicals
3-Pyridinecarboxylicacid,6-iodo-,methylester 96%
250mg
$ 61.00

Total 13 raw suppliers

Chemical Property of Methyl 6-iodonicotinate

Chemical Property:

Boiling Point:287.7±25.0 °C(Predicted)
PKA:-0.19±0.10(Predicted)
PSA：39.19000
Density:1.844±0.06 g/cm3(Predicted)
LogP:1.47280
Storage Temp.:under inert gas (nitrogen or Argon) at 2–8 °C
XLogP3:1.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:262.94433
Heavy Atom Count:11
Complexity:151

Purity/Quality:

97% ^*data from raw suppliers

Methyl6-iodonicotinate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC(=O)C1=CN=C(C=C1)I

Technology Process of Methyl 6-iodonicotinate

There total 2 articles about Methyl 6-iodonicotinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-iodo-nicotinic acid: 13054-02-9
6-iodo-nicotinic acid

: 18107-18-1
diazomethyl-trimethyl-silane

: 173157-33-0
methyl 6-iodo-3-pyridinecarboxylate

Guidance literature:: In methanol; toluene; at 0 - 20 ℃; for 2h;

Reference yield:

: 163276-23-1
methyl 2-<(trifluoromethyl)sulfonyl>pyridine-5-carboxylate

: 173157-33-0
methyl 6-iodo-3-pyridinecarboxylate

Guidance literature:: methyl 2-<(trifluoromethyl)sulfonyl>pyridine-5-carboxylate; With hydrogenchloride; sodium iodide; In diethyl ether; toluene; at 20 - 40 ℃;

With sodium hydroxide; In diethyl ether; water; toluene; at 5 ℃; pH=10;
DOI:10.1021/jo900726f

Reference yield: 100.0%

: 20541-49-5
bis(p-chlorophenyl) diselenide

: 173157-33-0
methyl 6-iodo-3-pyridinecarboxylate

: 6-(4-chloro-phenylselanyl)-nicotinic acid methyl ester

Guidance literature:: With polymer supported borohydride; bis(bipyridine)nickel(II) bromide; In methanol; at 60 ℃; for 16h;
DOI:10.1021/ol0058184