7-Boc-7-azaspiro[3.5]nonane-2-Methanol

Base Information

• Chemical Name: 7-Boc-7-azaspiro[3.5]nonane-2-Methanol
• CAS No.: 1356476-27-1
• Molecular Formula: C₁₄H₂₅NO₃
• Molecular Weight: 255.357
• Hs Code.: 2933990090
• Mol file: 1356476-27-1.mol

Synonyms:7-Boc-7-azaspiro[3.5]nonane-2-Methanol;tert-butyl 2-(hydroxymethyl)-7-azaspiro[3.5]nonane-7-carboxylate;2-(hydroxymethyl)-7-Azaspiro[3.5]nonane-7-carboxylic acid 1,1-dimethylethyl ester

Chemical Property of 7-Boc-7-azaspiro[3.5]nonane-2-Methanol

Chemical Property:

• Boiling Point: 364.6±15.0 °C(Predicted)
• PKA: 14.97±0.10(Predicted)
• PSA: 49.77000
• Density: 1.10±0.1 g/cm3(Predicted)
• LogP: 2.34390
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

tert-butyl2-(hydroxymethyl)-7-azaspiro[3.5]nonane-7-carboxylate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 7-Boc-7-azaspiro[3.5]nonane-2-Methanol

There total 1 articles about 7-Boc-7-azaspiro[3.5]nonane-2-Methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + tert-butyl 2-iodo-7-azaspiro[3.5]nonane-7-carboxylate → 2-(hydroxymethyl)-7-azaspiro[3.5]decane-7-carboxylic acid tert-butyl ester (1356476-27-1)

Guidance literature:

With (4s,6s)-2,4,5,6-tetra(9H-carbazol-9-yl)isophthalonitrile; N-ethyl-N,N-diisopropylamine; In water; acetonitrile; at 20 ℃; for 16h; Irradiation;

DOI:10.1039/d1sc03083c

upstream raw materials:

formaldehyd

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