5-Iodo-2,3-dihydro-1H-indene

Base Information

Chemical Name:5-Iodo-2,3-dihydro-1H-indene
CAS No.:132464-83-6
Molecular Formula:C9H7I
Molecular Weight:244.07
Hs Code.:2903999090
European Community (EC) Number:826-687-4
DSSTox Substance ID:DTXSID30567974
Nikkaji Number:J1.802.449G
Wikidata:Q82454055
Mol file:132464-83-6.mol

Synonyms:5-Iodo-2,3-dihydro-1H-indene;132464-83-6;5-Iodoindane;1H-Indene, 2,3-dihydro-5-iodo-;SCHEMBL4525476;DTXSID30567974;CS-B0805;MFCD09842510;AKOS009319652;CS-14673;EN300-197278;Z381540774

Suppliers and Price of 5-Iodo-2,3-dihydro-1H-indene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
5-Iodo-2,3-dihydro-1H-indene
500mg
$ 175.00

Matrix Scientific
5-Iodoindane 97%
1g
$ 249.00

Crysdot
5-Iodo-2,3-dihydro-1H-indene 95+%
1g
$ 313.00

Chemenu
5-iodo-2,3-dihydro-1H-indene 95%
1g
$ 296.00

Atlantic Research Chemicals
5-Iodoindane 95%
1gm:
$ 258.02

American Custom Chemicals Corporation
5-IODOINDANE 95.00%
5MG
$ 499.99

Alichem
5-Iodo-2,3-dihydro-1H-indene
1g
$ 267.75

AK Scientific
5-Iodoindane
1g
$ 386.00

Total 7 raw suppliers

Chemical Property of 5-Iodo-2,3-dihydro-1H-indene

Chemical Property:

PSA：0.00000
LogP:2.77990
Storage Temp.:2-8°C
XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:0
Exact Mass:243.97490
Heavy Atom Count:10
Complexity:122

Purity/Quality:

≥95% ^*data from raw suppliers

5-Iodo-2,3-dihydro-1H-indene ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC2=C(C1)C=C(C=C2)I

Technology Process of 5-Iodo-2,3-dihydro-1H-indene

There total 1 articles about 5-Iodo-2,3-dihydro-1H-indene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 24425-40-9
indan-5-amine

: 132464-83-6
2,3-dihydro-5-iodo-1H-indene

Guidance literature:: With hydrogenchloride; potassium iodide; sodium nitrite; In water; at 0 - 5 ℃; for 2h;
DOI:10.1016/j.bmcl.2019.126838

Reference yield:

: 132464-83-6
2,3-dihydro-5-iodo-1H-indene

: 132464-80-3
4-(2-Chloro-phenyl)-2-(2-indan-5-yl-ethyl)-9-methyl-6H-1-thia-5,7,8,9a-tetraaza-cyclopenta[e]azulene

Guidance literature:: Multi-step reaction with 4 steps

1: Ph₃P, CuI, Et₃N, palladium acetate / acetonitrile / 2 h / Ambient temperature

2: K₂CO₃ / methanol / 2 h / Ambient temperature

3: 67 percent / Ph₃P, CuI, Et₃N, palladium acetate / dimethylformamide / 5 h

4: 43 percent / H₂ / 5percent Pd/C / ethanol; tetrahydrofuran / 5 h / 760 Torr

With copper(l) iodide; hydrogen; palladium diacetate; potassium carbonate; triethylamine; triphenylphosphine; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm00108a031

Reference yield:

: 132464-83-6
2,3-dihydro-5-iodo-1H-indene

: 132464-76-7
4-(2-Chloro-phenyl)-2-((Z)-2-indan-5-yl-vinyl)-9-methyl-6H-1-thia-5,7,8,9a-tetraaza-cyclopenta[e]azulene

Guidance literature:: Multi-step reaction with 4 steps

1: Ph₃P, CuI, Et₃N, palladium acetate / acetonitrile / 2 h / Ambient temperature

2: K₂CO₃ / methanol / 2 h / Ambient temperature

3: 67 percent / Ph₃P, CuI, Et₃N, palladium acetate / dimethylformamide / 5 h

4: 52 percent / H₂, thiophene / 5percent Pd/C / ethanol; tetrahydrofuran / 2 h / 760 Torr

With thiophene; copper(l) iodide; hydrogen; palladium diacetate; potassium carbonate; triethylamine; triphenylphosphine; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm00108a031