methyl 4,6,7-trimethoxy-5-(methoxymethoxy)naphthalene-2-carboxylate

Base Information

Chemical Name:methyl 4,6,7-trimethoxy-5-(methoxymethoxy)naphthalene-2-carboxylate
CAS No.:104197-39-9
Molecular Formula:C₁₇H₂₀O₇
Molecular Weight:336.342
Hs Code.:
Mol file:104197-39-9.mol

Synonyms:2-Naphthalenecarboxylic acid, 4,6,7-triMethoxy-5-(MethoxyMethoxy)-, Methyl ester

Suppliers and Price of methyl 4,6,7-trimethoxy-5-(methoxymethoxy)naphthalene-2-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of methyl 4,6,7-trimethoxy-5-(methoxymethoxy)naphthalene-2-carboxylate

Chemical Property:

Vapor Pressure:7.23E-09mmHg at 25°C
Boiling Point:466.2°C at 760 mmHg
Flash Point:205.3°C
Density:1.199g/cm³

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of methyl 4,6,7-trimethoxy-5-(methoxymethoxy)naphthalene-2-carboxylate

There total 2 articles about methyl 4,6,7-trimethoxy-5-(methoxymethoxy)naphthalene-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 104197-38-8
4-Hydroxy-6,7-dimethoxy-5-methoxymethoxy-naphthalene-2-carboxylic acid methyl ester

: 77-78-1
dimethyl sulfate

: 104197-39-9
4,6,7-Trimethoxy-5-methoxymethoxy-naphthalene-2-carboxylic acid methyl ester

Guidance literature:: DOI:10.1021/jo00370a037

Reference yield:

: 104197-37-7
6,7-Dimethoxy-5-methoxymethoxy-4-oxo-1,2,3,4-tetrahydro-naphthalene-2-carboxylic acid methyl ester

: 104197-39-9
4,6,7-Trimethoxy-5-methoxymethoxy-naphthalene-2-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) LDA, 2.) phenyl selenium bromide

2: 71 percent

With Phenylselenyl bromide; lithium diisopropyl amide;
DOI:10.1021/jo00370a037