2-AMINO-4-(3-NITROPHENYL)-5-THIAZOLECARBOXYLIC ACID ETHYL ESTER

Base Information

Chemical Name:2-AMINO-4-(3-NITROPHENYL)-5-THIAZOLECARBOXYLIC ACID ETHYL ESTER
CAS No.:172848-42-9
Molecular Formula:C12H11N3O4S
Molecular Weight:0
Hs Code.:
Mol file:172848-42-9.mol

Synonyms:2-AMINO-4-(3-NITROPHENYL)-5-THIAZOLECARBOXYLIC ACID ETHYL ESTER

Suppliers and Price of 2-AMINO-4-(3-NITROPHENYL)-5-THIAZOLECARBOXYLIC ACID ETHYL ESTER

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 2-AMINO-4-(3-NITROPHENYL)-5-THIAZOLECARBOXYLIC ACID ETHYL ESTER

Chemical Property:

Melting Point:228 - 230 °C (ethanol)
PSA：139.27000
LogP:3.58160

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-AMINO-4-(3-NITROPHENYL)-5-THIAZOLECARBOXYLIC ACID ETHYL ESTER

There total 5 articles about 2-AMINO-4-(3-NITROPHENYL)-5-THIAZOLECARBOXYLIC ACID ETHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 65573-12-8
4-chloro-5H-1,2,3-dithiazole-5-one

: 247242-37-1
ethyl 3-amino-3-(3-nitrophenyl)-2-propenoate

: 172848-42-9
2-amino-5-ethoxycarbonyl-4-(3-nitrophenyl)thiazole

: 4-(3-nitro-phenyl)-2-oxo-2,3-dihydro-thiazole-5-carboxylic acid ethyl ester

Guidance literature:: In dimethyl sulfoxide; at 120 ℃; for 5h;
DOI:10.1016/S0040-4039(99)01235-6

Reference yield:

: 52119-38-7
ethyl 3-oxo-3-(3-nitrophenyl)propanoate

: 27126-76-7
[hydroxy(tosyloxy)iodo]benzene

: 172848-42-9
2-amino-5-ethoxycarbonyl-4-(3-nitrophenyl)thiazole

Guidance literature:: With thiourea; In ethyl acetate; acetonitrile;

Reference yield:

: 52119-38-7
ethyl 3-oxo-3-(3-nitrophenyl)propanoate

: 172848-42-9
2-amino-5-ethoxycarbonyl-4-(3-nitrophenyl)thiazole

Guidance literature:: Multi-step reaction with 2 steps

1: pyridinium bromide perbromide, HBr / acetic acid / 0.5 h / Ambient temperature

2: ethanol / 0.5 h / Heating

With hydrogen bromide; pyridinium hydrobromide perbromide; In ethanol; acetic acid;