2-(Iodomethyl)-1-(phenylsulfonyl)aziridine

Base Information

Chemical Name:2-(Iodomethyl)-1-(phenylsulfonyl)aziridine
CAS No.:6453-90-3
Molecular Formula:C₉H₁₀INO₂S
Molecular Weight:323.154
Hs Code.:
NSC Number:122001
DSSTox Substance ID:DTXSID90298252,DTXSID20983700

Synonyms:6453-90-3;2-(iodomethyl)-1-(phenylsulfonyl)aziridine;1-(benzenesulfonyl)-2-(iodomethyl)aziridine;NSC122001;DTXSID20983700;DTXSID90298252;NSC-122001

Suppliers and Price of 2-(Iodomethyl)-1-(phenylsulfonyl)aziridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2-(Iodomethyl)-1-(phenylsulfonyl)aziridine

Chemical Property:

Vapor Pressure:9.14E-07mmHg at 25°C
Boiling Point:404.9°Cat760mmHg
Flash Point:198.7°C
Density:1.884g/cm³
XLogP3:2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:322.94770
Heavy Atom Count:14
Complexity:292

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C(N1S(=O)(=O)C2=CC=CC=C2)CI

Technology Process of 2-(Iodomethyl)-1-(phenylsulfonyl)aziridine

There total 2 articles about 2-(Iodomethyl)-1-(phenylsulfonyl)aziridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 50487-70-2
N-allylbenzenesulfonamide

: 6453-90-3
2-(iodomethyl)-1-(phenylsulfonyl)aziridine

Guidance literature:: N-allylbenzenesulfonamide; With sodium hydride; In diethyl ether; at 20 ℃; for 0.333333h; Inert atmosphere;

With iodine; In diethyl ether; at 20 ℃; for 16h; Inert atmosphere; Darkness;
DOI:10.1021/jacs.1c04180

Reference yield:

: 98-09-9
benzenesulfonyl chloride

: 6453-90-3
2-(iodomethyl)-1-(phenylsulfonyl)aziridine

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 0 - 20 °C

2: sodium iodide; tert-butylhypochlorite / acetonitrile

With tert-butylhypochlorite; triethylamine; sodium iodide; In dichloromethane; acetonitrile;
DOI:10.1002/ejoc.202000537