3,3'-Dithiobis(benzoic acid chloride)

Base Information

• Chemical Name: 3,3'-Dithiobis(benzoic acid chloride)
• CAS No.: 69384-66-3
• Molecular Formula: C14H8Cl2O2S2
• Molecular Weight: 343.254
• Mol file: 69384-66-3.mol

Synonyms:3,3'-Dithiobis(benzoic acid chloride)

Chemical Property of 3,3'-Dithiobis(benzoic acid chloride)

Chemical Property:

• PSA: 84.74000
• LogP: 5.24400

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,3'-Dithiobis(benzoic acid chloride)

There total 3 articles about 3,3'-Dithiobis(benzoic acid chloride) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

3,3'-dithiobis-benzoic acid (1227-49-2) → 3,3'-disulfanediyldibenzoyl dichloride (69384-66-3)

Guidance literature:

With thionyl chloride; N,N-dimethyl-formamide; In toluene; at 70 ℃; for 4h;

Reference yield:

triethylammonium hemi(3,3'-disulfanediyldibenzoate) → 3,3'-disulfanediyldibenzoyl dichloride (69384-66-3)

Guidance literature:

With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 20 ℃; for 5h;

DOI:10.1055/s-2008-1067102

Reference yield:

→ 3,3'-disulfanediyldibenzoyl dichloride (69384-66-3)

Guidance literature:

Disulfid (IV), PCl5;

upstream raw materials:

3,3'-dithiobis-benzoic acid

Downstream raw materials:

3,3'-disulfanediyl-di-benzoic acid-dianilide

bis(3-(dimethylaminomethyl)phenyl) disulfide

C₂₂H₂₄N₂O₄S₂

3,3'-dithiodibenzamide