3,3'-dithiodibenzamide

Base Information

• Chemical Name: 3,3'-dithiodibenzamide
• CAS No.: 107920-19-4
• Molecular Formula: C₁₄H₁₂N₂O₂S₂
• Molecular Weight: 304.393
• Mol file: 107920-19-4.mol

Synonyms:3,3'-dithiodibenzamide

Chemical Property of 3,3'-dithiodibenzamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,3'-dithiodibenzamide

There total 2 articles about 3,3'-dithiodibenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

3,3'-disulfanediyldibenzoyl dichloride (69384-66-3) → 3,3'-dithiodibenzamide (107920-19-4)

Guidance literature:

With ammonia; In tetrahydrofuran; at 0 - 20 ℃; for 10h; Green chemistry;

Reference yield:

3,3'-dithiobis-benzoic acid (1227-49-2) → 3,3'-dithiodibenzamide (107920-19-4)

Guidance literature:

With thionyl chloride; iron(III) chloride; Behandeln des Reaktionsprodukts mit wss. Ammoniak;

DOI:10.1039/jr9300001095

Reference yield:

3,3'-dithiodibenzamide (107920-19-4) → 3-(4,5-dihydro-1H-imidazol-2-yl)-thiophenol (872276-84-1)

Guidance literature:

Multi-step reaction with 2 steps

1: phosphorus (V)-oxide; xylene

2: ethanol; H₂S / unter Druck

With ethanol; hydrogen sulfide; phosphorus pentoxide; xylene;

DOI:10.1039/jr9300001095

upstream raw materials:

3,3'-dithiobis-benzoic acid

3,3'-disulfanediyldibenzoyl dichloride

Downstream raw materials:

3,3'-disulfanediyl-di-benzonitrile

3-(4,5-dihydro-1H-imidazol-2-yl)-thiophenol

bis-[3-(4,5-dihydro-1H-imidazol-2-yl)-phenyl]-disulfide