Ethyl 2-oxocyclotridecanecarboxylate

Base Information

Chemical Name:Ethyl 2-oxocyclotridecanecarboxylate
CAS No.:22591-34-0
Molecular Formula:C₁₆H₂₈O₃
Molecular Weight:268.397
Hs Code.:
DSSTox Substance ID:DTXSID10447780
Mol file:22591-34-0.mol

Synonyms:Ethyl 2-oxocyclotridecanecarboxylate;AGN-PC-0NCILO;SCHEMBL7733726;DTXSID10447780;AKOS024318973;22591-34-0

Suppliers and Price of Ethyl 2-oxocyclotridecanecarboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Ethyl 2-oxocyclotridecanecarboxylate

Chemical Property:

XLogP3:5.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:268.20384475
Heavy Atom Count:19
Complexity:273

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C1CCCCCCCCCCCC1=O

Technology Process of Ethyl 2-oxocyclotridecanecarboxylate

There total 5 articles about Ethyl 2-oxocyclotridecanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 623-73-4
diazoacetic acid ethyl ester

: 830-13-7
cyclododecanone

: 58643-74-6,22591-34-0
ethyl 2-oxocyclotridecanecarboxylate

Guidance literature:: With triethyloxonium fluoroborate; In dichloromethane;
DOI:10.1002/hlca.19750580821

Reference yield:

: Diazo-(1-hydroxy-cyclododecyl)-acetic acid ethyl ester

: 58643-74-6,22591-34-0
ethyl 2-oxocyclotridecanecarboxylate

Guidance literature:: With hydrogenchloride; In pentane;

Reference yield:

: 830-13-7
cyclododecanone

: 58643-74-6,22591-34-0
ethyl 2-oxocyclotridecanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: nBuLi

2: HCl / pentane

With hydrogenchloride; n-butyllithium; In pentane;