3,4,5-TRIFLUOROPHENACYL BROMIDE

Base Information

Chemical Name:3,4,5-TRIFLUOROPHENACYL BROMIDE
CAS No.:443914-94-1
Molecular Formula:C8H4BrF3O
Molecular Weight:253.02
Hs Code.:2914700090
Mol file:443914-94-1.mol

Synonyms:3,4,5-TRIFLUOROPHENACYL BROMIDE;2-Bromo-3',4',5'-trifluoroacetophenone, 2-Bromo-1-(3,4,5-trifluorophenyl)ethan-1-one;2-bromo-1-(3,4,5-trifluorophenyl)ethanone

Suppliers and Price of 3,4,5-TRIFLUOROPHENACYL BROMIDE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

SynQuest Laboratories
3,4,5-Trifluorophenacyl bromide
5 g
$ 384.00

SynQuest Laboratories
3,4,5-Trifluorophenacyl bromide
1 g
$ 144.00

Crysdot
2-Bromo-1-(3,4,5-trifluorophenyl)ethanone 97%
5g
$ 594.00

American Custom Chemicals Corporation
3,4,5-TRIFLUOROPHENACYL BROMIDE 95.00%
5G
$ 1367.52

American Custom Chemicals Corporation
3,4,5-TRIFLUOROPHENACYL BROMIDE 95.00%
1G
$ 791.18

Total 2 raw suppliers

Chemical Property of 3,4,5-TRIFLUOROPHENACYL BROMIDE

Chemical Property:

PSA：17.07000
LogP:2.68150

Purity/Quality:

97% ^*data from raw suppliers

3,4,5-Trifluorophenacyl bromide ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:T

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3,4,5-TRIFLUOROPHENACYL BROMIDE

There total 3 articles about 3,4,5-TRIFLUOROPHENACYL BROMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 220141-73-1
1-(3,4,5-trifluorophenyl)ethanone

: 443914-94-1
2-bromo-1-(3,4,5-trifluorophenyl)ethan-1-one

Guidance literature:: With dioxane dibromide; In 1,4-dioxane; diethyl ether; at 20 ℃; for 2h;
DOI:10.1021/acs.inorgchem.1c02121

Reference yield: 57.0%

: 69739-34-0
t-butyldimethylsiyl triflate

: 1-(3,4,5-trifluorophenyl)ethanone

: 443914-94-1
2-bromo-1-(3,4,5-trifluorophenyl)ethan-1-one

Guidance literature:: t-butyldimethylsiyl triflate; 1-(3,4,5-trifluorophenyl)ethanone; With triethylamine; In dichloromethane; at 20 ℃; for 1h;

With N-Bromosuccinimide; In tetrahydrofuran; water; at 20 ℃; for 0.25h;

Reference yield:

: 138526-69-9
3,4,5-trifluoro-1-bromobenzene

: 443914-94-1
2-bromo-1-(3,4,5-trifluorophenyl)ethan-1-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: magnesium; iodine / tetrahydrofuran / 0.5 h / 20 °C

1.2: 1 h / 0 °C

2.1: hydrogen bromide; bromine / chloroform / 1 h / 20 °C

With hydrogen bromide; bromine; iodine; magnesium; In tetrahydrofuran; chloroform;