N-(4-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)pyridin-2-yl)propionaMide

Base Information

Chemical Name:N-(4-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)pyridin-2-yl)propionaMide
CAS No.:1285530-34-8
Molecular Formula:C14H21BN2O3
Molecular Weight:276.143
Hs Code.:
Mol file:1285530-34-8.mol

Synonyms:N-(4-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)pyridin-2-yl)propionaMide;2-Propionamidopyridine-4-boronic acid pinacol ester

Suppliers and Price of N-(4-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)pyridin-2-yl)propionaMide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
2-Propionamidopyridine-4-boronic acid pinacol ester Aldrich
1g
$ 541.00

Crysdot
N-(4-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)pyridin-2-yl)propionamide 95+%
1g
$ 904.00

American Custom Chemicals Corporation
2-PROPIONAMIDOPYRIDINE-4-BORONIC ACID PINACOL ESTER 95.00%
1G
$ 910.35

American Custom Chemicals Corporation
2-PROPIONAMIDOPYRIDINE-4-BORONIC ACID PINACOL ESTER 95.00%
5MG
$ 496.35

Total 3 raw suppliers

Chemical Property of N-(4-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)pyridin-2-yl)propionaMide

Chemical Property:

PSA：60.45000
LogP:1.80230

Purity/Quality:

99% ^*data from raw suppliers

2-Propionamidopyridine-4-boronic acid pinacol ester Aldrich ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:T
Statements: 25
Safety Statements: 45

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-(4-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)pyridin-2-yl)propionaMide

There total 2 articles about N-(4-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)pyridin-2-yl)propionaMide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1285530-55-3
N-(4-bromopyridin-2-yl)propionamide

: 73183-34-3
bis(pinacol)diborane

: 1285530-34-8
N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridin-2-yl)propionamide

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; In 1,4-dioxane; at 100 ℃; for 0.5h; Microwave irradiation;

Reference yield:

: 84249-14-9
2-amino-4-bromopyridine

: 1285530-34-8
N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridin-2-yl)propionamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine / dichloromethane / 0.33 h / 20 °C

1.2: 20 °C

2.1: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 0.5 h / 100 °C / Microwave irradiation

With pyridine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; In 1,4-dioxane; dichloromethane;

Reference yield: 78.0%

: 1285530-34-8
N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridin-2-yl)propionamide

: 1338582-24-3
2-(4-fluorophenyl)-3-iodo-4,5,6,7-tetrahydropyrazolo[1,5-a]pyridine

: 1338580-85-0
N-{4-[2-(4-Fluorophenyl)-4,5,6,7-tetrahydropyrazolo[1,5-a]pyridin-3-yl]pyridin-2-yl}propanamide

Guidance literature:: With sodium carbonate; (bis(tricyclohexyl)phosphine)palladium(II) dichloride; In 1,4-dioxane; water; at 120 ℃; for 0.25h; Inert atmosphere; Microwave irradiation;