methyl 4-(acetyloxy)-5-methoxynaphthalene-2-carboxylate

Base Information

Chemical Name:methyl 4-(acetyloxy)-5-methoxynaphthalene-2-carboxylate
CAS No.:120016-55-9
Molecular Formula:C₁₅H₁₄O₅
Molecular Weight:274.273
Hs Code.:
Mol file:120016-55-9.mol

Synonyms:2-Naphthalenecarboxylic acid, 4-(acetyloxy)-5-Methoxy-, Methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 4-(acetyloxy)-5-methoxynaphthalene-2-carboxylate

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:428.479°C at 760 mmHg
Flash Point:191.231°C
Density:1.23g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of methyl 4-(acetyloxy)-5-methoxynaphthalene-2-carboxylate

There total 1 articles about methyl 4-(acetyloxy)-5-methoxynaphthalene-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 115061-22-8
methyl 4-acetoxy-8-bromo-5-methoxynaphthalene-2-carboxylate

: 120016-55-9
4-acetoxy-5-methoxy-[2]naphthoic acid methyl ester

Guidance literature:: With hydrogen; potassium acetate; palladium on activated charcoal; In ethanol; ethyl acetate;

Reference yield: 96.0%

: 120016-55-9
4-acetoxy-5-methoxy-[2]naphthoic acid methyl ester

: 93087-61-7
methyl 4-hydroxy-5-methoxynaphthalene-2-carboxylate

Guidance literature:: With sodium methylate; In methanol; for 0.5h;
DOI:10.1071/C97190

Reference yield:

: 120016-55-9
4-acetoxy-5-methoxy-[2]naphthoic acid methyl ester

: 3785-24-8
nepodin

Guidance literature:: Multi-step reaction with 5 steps

1: 95 percent / LiAlH₄ / tetrahydrofuran / 1 h / Ambient temperature

2: 98 percent / H₂, conc. HCl / 10percent Pd/C / ethanol

3: pyridine / 24 h / Ambient temperature

4: 74 percent / BF₃*Et₂O / 1 h / 60 °C

5: 85 percent / BCl₃ / CH₂Cl₂ / 23 h / Ambient temperature

With pyridine; hydrogenchloride; lithium aluminium tetrahydride; boron trifluoride diethyl etherate; hydrogen; boron trichloride; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane;