3-[[(1,1-DiMethylethyl)di...

Base Information

• Chemical Name: 3-[[(1,1-DiMethylethyl)di...
• CAS No.: 929913-18-8
• Molecular Formula: C10H20O2Si
• Molecular Weight: 200.353
• Hs Code.: 2931900090
• Mol file: 929913-18-8.mol

Synonyms:3-[[(1,1-DiMethylethyl)diMethylsilyl]oxy]cyclobutanone;3-[(tert-butyldimethylsilyl)oxy]cyclobutan-1-one;3-((tert-Butyldimethylsilyl)oxy)cyclobutanone

Chemical Property of 3-[[(1,1-DiMethylethyl)di...

Chemical Property:

• Boiling Point: 219.9±33.0 °C(Predicted)
• PSA: 26.30000
• Density: 0.93±0.1 g/cm3(Predicted)
• LogP: 2.73970
• Storage Temp.: Sealed in dry,Store in freezer, under -20°C

Purity/Quality:

97% ^*data from raw suppliers

3-[[(1,1-Dimethylethyl)dimethylsilyl]oxy]cyclobutanone ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 3-[[(1,1-Dimethylethyl)dimethylsilyl]oxy]cyclobutanone can be used as a cardiac sarcomere inhibitor.

Technology Process of 3-[[(1,1-DiMethylethyl)di...

There total 4 articles about 3-[[(1,1-DiMethylethyl)di... which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

2,2-dichloro-3-tert-butyldimethylsilyloxycyclobutanone (929911-60-4) → 3-((tert-butyldimethylsilyl)oxy)cyclobutan-1-one (929913-18-8)

Guidance literature:

With zinc/copper couple; ammonium chloride; In methanol; at 20 ℃; for 24h;

Reference yield:

3-((tert-butyl dimethylsilyl)oxy)cyclobutan-1-ol (1089709-08-9,1408074-89-4,1408075-44-4) → 3-((tert-butyldimethylsilyl)oxy)cyclobutan-1-one (929913-18-8)

Guidance literature:

With sodium hydrogencarbonate; Dess-Martin periodane; In dichloromethane; at 20 ℃; for 4h;

Reference yield:

3-hydroxycyclobutan-1-one (15932-93-1) + tert-butyldimethylsilyl chloride (18162-48-6) → 3-((tert-butyldimethylsilyl)oxy)cyclobutan-1-one (929913-18-8)

Guidance literature:

With 1H-imidazole; In N,N-dimethyl-formamide; at 0 - 30 ℃; for 18h; Inert atmosphere;

upstream raw materials:

2,2-dichloro-3-tert-butyldimethylsilyloxycyclobutanone

3-((tert-butyl dimethylsilyl)oxy)cyclobutan-1-ol

3-hydroxycyclobutan-1-one

tert-butyldimethylsilyl chloride

Downstream raw materials:

(1s,3s)-3-((tert-butyldimethylsilyl)oxy)cyclobutanol

3-tert-butyldimethylsiloxy-3',4'-dihydrospirocyclobutane-1,2'-pyrano[2,3-c]pyridin-4'-one

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