1H-1,4-Diazepin-6-amine,hexahydro-1-methyl-4-(1-methylethyl)-(9CI)

Base Information

Chemical Name:1H-1,4-Diazepin-6-amine,hexahydro-1-methyl-4-(1-methylethyl)-(9CI)
CAS No.:483303-70-4
Molecular Formula:C₉H₂₁N₃
Molecular Weight:171.286
Hs Code.:
Mol file:483303-70-4.mol

Synonyms:1H-1,4-Diazepin-6-amine,hexahydro-1-methyl-4-(1-methylethyl)-(9CI)

Suppliers and Price of 1H-1,4-Diazepin-6-amine,hexahydro-1-methyl-4-(1-methylethyl)-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 1H-1,4-Diazepin-6-amine,hexahydro-1-methyl-4-(1-methylethyl)-(9CI)

Chemical Property:

PSA：32.50000
LogP:0.54560

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1H-1,4-Diazepin-6-amine,hexahydro-1-methyl-4-(1-methylethyl)-(9CI)

There total 5 articles about 1H-1,4-Diazepin-6-amine,hexahydro-1-methyl-4-(1-methylethyl)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 483303-68-0
1-isopropyl-4-methyl-6-nitrohexahydro-1,4-diazepine

: 483303-70-4
6-amino-1-isopropyl-4-methylhexahydro-1,4-diazepine

Guidance literature:: With hydrogen; nickel; In ethanol; at 20 ℃; for 3h;
DOI:10.1248/cpb.50.941

Reference yield:

: 109-56-8
i-propyl(2-(hydroxy)ethyl)amine

: 483303-70-4
6-amino-1-isopropyl-4-methylhexahydro-1,4-diazepine

Guidance literature:: Multi-step reaction with 5 steps

1.1: 99 percent / SOCl₂ / CHCl₃ / 6 h / Heating

2.1: 29 percent / ethanol; H₂O / 16 h / 50 °C

3.1: aq. NaHCO₃ / 2 h / 40 - 50 °C

4.1: t-BuOK / methanol / 0.5 h / 50 °C

4.2: NH₂OH*HCl / H₂O

5.1: H₂ / Raney-Ni / ethanol / 3 h / 20 °C

With thionyl chloride; potassium tert-butylate; hydrogen; sodium hydrogencarbonate; nickel; In methanol; ethanol; chloroform; water;
DOI:10.1248/cpb.50.941

Reference yield:

: 146981-02-4
N-isopropyl-N'-methylethylenediamine

: 483303-70-4
6-amino-1-isopropyl-4-methylhexahydro-1,4-diazepine

Guidance literature:: Multi-step reaction with 3 steps

1.1: aq. NaHCO₃ / 2 h / 40 - 50 °C

2.1: t-BuOK / methanol / 0.5 h / 50 °C

2.2: NH₂OH*HCl / H₂O

3.1: H₂ / Raney-Ni / ethanol / 3 h / 20 °C

With potassium tert-butylate; hydrogen; sodium hydrogencarbonate; nickel; In methanol; ethanol;
DOI:10.1248/cpb.50.941