3-Iodomethyl-1-cyclohexene

Base Information

Chemical Name:3-Iodomethyl-1-cyclohexene
CAS No.:34825-94-0
Molecular Formula:C7H11I
Molecular Weight:222.07
Hs Code.:
Mol file:34825-94-0.mol

Synonyms:3-Iodomethyl-1-cyclohexene

Suppliers and Price of 3-Iodomethyl-1-cyclohexene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 3-Iodomethyl-1-cyclohexene

Chemical Property:

Boiling Point:85 °C (10 mmHg)
PSA：0.00000
LogP:2.77770

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-Iodomethyl-1-cyclohexene

There total 6 articles about 3-Iodomethyl-1-cyclohexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 7432-49-7,6376-96-1,31022-87-4,38263-37-5,38263-38-6,136616-41-6
endo-2-norcaranol

: 34825-94-0
3-(iodomethyl)-1-cyclohexene

Guidance literature:: With magnesium iodide; zinc(II) iodide; In diethyl ether; for 4h; Heating;
DOI:10.1021/jo01301a003

Reference yield: 96.0%

: 4109-94-8
(iodomethyl)zinc iodide

: 1521-51-3,113667-32-6
rac-3-bromocyclohexene

: 34825-94-0
3-(iodomethyl)-1-cyclohexene

Guidance literature:: With CuI*2LiI; In tetrahydrofuran; at -20 - -10 ℃; Product distribution; other electrophiles (acyl chlorides, enones, aldehydes, allyl bromides) and copper and zinc carbenoids;
DOI:10.1021/jo00283a006

Reference yield: 88.0%

: 930-68-7
cyclohexenone

: 75-11-6
diiodomethane

: 34825-94-0
3-(iodomethyl)-1-cyclohexene

Guidance literature:: cyclohexenone; diiodomethane; With methyllithium lithium bromide; In tetrahydrofuran; at -78 ℃; for 0.75h; Inert atmosphere;

With hexylsilane; tris(pentafluorophenyl)borate; In dichloromethane; at 20 ℃; for 1h; chemoselective reaction; Inert atmosphere;
DOI:10.1021/acs.orglett.0c02831