Phenol, 4-[(1E)-2-(4-hydroxyphenyl)-1,2-diphenylethenyl]- Phenol, 4,4'-(1,2-diphenyl-1,2-ethenediyl)bis-, (E)- (9CI)

Base Information

• Chemical Name: Phenol, 4-[(1E)-2-(4-hydroxyphenyl)-1,2-diphenylethenyl]- Phenol, 4,4'-(1,2-diphenyl-1,2-ethenediyl)bis-, (E)- (9CI)
• CAS No.: 80232-65-1
• Molecular Formula: C26H20O2
• Molecular Weight: 364.444
• Mol file: 80232-65-1.mol

Synonyms:Phenol, 4-[(1E)-2-(4-hydroxyphenyl)-1,2-diphenylethenyl]- Phenol, 4,4'-(1,2-diphenyl-1,2-ethenediyl)bis-, (E)- (9CI);(E)-4,4'-(1,2-diphenylethene-1,2-diyl)diphenol;1,2-bis(4-hydroxyphenyl)-1,2-diphenylethene

Chemical Property of Phenol, 4-[(1E)-2-(4-hydroxyphenyl)-1,2-diphenylethenyl]- Phenol, 4,4'-(1,2-diphenyl-1,2-ethenediyl)bis-, (E)- (9CI)

Chemical Property:

• Boiling Point: 488.8±40.0 °C(Predicted)
• PKA: 9.89±0.15(Predicted)
• PSA: 40.46000
• Density: 1.205±0.06 g/cm3(Predicted)
• LogP: 6.10520

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Phenol, 4-[(1E)-2-(4-hydroxyphenyl)-1,2-diphenylethenyl]- Phenol, 4,4'-(1,2-diphenyl-1,2-ethenediyl)bis-, (E)- (9CI)

There total 13 articles about Phenol, 4-[(1E)-2-(4-hydroxyphenyl)-1,2-diphenylethenyl]- Phenol, 4,4'-(1,2-diphenyl-1,2-ethenediyl)bis-, (E)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

1,2-bis-(4-methoxyphenyl)-1,2-diphenylethene (68578-78-9) → (E/Z)-1,2-bis-(4-hydroxyphenyl)-1,2-diphenylethylene (80232-65-1,68578-79-0)

Guidance literature:

1,2-bis-(4-methoxyphenyl)-1,2-diphenylethene; With boron tribromide; In dichloromethane; at 0 - 20 ℃; for 22.5h;

With water; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1039/c5tc01597a

Reference yield: 97.0%

trans-1,2-di(4-methoxyphenyl)-1,2-diphenylethylene (70592-03-9,68578-78-9) → 4,4′-(1,2-diphenylethene-1,2-diyl)diphenol (80232-65-1)

Guidance literature:

With boron tribromide; In dichloromethane; at -78 - 20 ℃;

DOI:10.1039/c5cc02377g

Reference yield: 86.0%

4-Hydroxybenzophenone (1137-42-4) → (E/Z)-1,2-bis-(4-hydroxyphenyl)-1,2-diphenylethylene (80232-65-1,68578-79-0)

Guidance literature:

With titanium tetrachloride; zinc; In tetrahydrofuran; at -78 ℃; Inert atmosphere; Reflux;

DOI:10.1002/anie.201507236

upstream raw materials:

α,α'-Bis(4-benzoyloxyphenyl)-stilben

benzophenone

4-Hydroxybenzophenone

<4-(Benzoyloxy)phenyl>phenylketon

Downstream raw materials:

C₄₄H₅₂O₈

C₄₈H₅₂O₄

C₃₈H₃₂O₄

C₄₂H₅₂O₁₀

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