4,4-Dimethoxytetrahydropyran-3-one

Base Information

Chemical Name:4,4-Dimethoxytetrahydropyran-3-one
CAS No.:693245-80-6
Molecular Formula:C7H12O4
Molecular Weight:160.17
Hs Code.:2932999099
European Community (EC) Number:888-157-9
Mol file:693245-80-6.mol

Synonyms:693245-80-6;4,4-dimethoxyoxan-3-one;4,4-DIMETHOXYTETRAHYDROPYRAN-3-ONE;4,4-DIMETHOXYDIHYDRO-2H-PYRAN-3(4H)-ONE;2H-Pyran-3(4H)-one,dihydro-4,4-dimethoxy-(9CI);2H-Pyran-3(4H)-one, dihydro-4,4-dimethoxy-;SCHEMBL1710129;VSYYQDBTLGSLRK-UHFFFAOYSA-N;AMY34906;MFCD18814922;AKOS025289858;PB16838;AS-51350;CS-0051118;FT-0758560;2h-pyran-3(4h)-one,dihydro-4,4-dimethoxy-;EN300-105244;P12465;4,4-Dimethoxytetrahydropyran-3-one, AldrichCPR;A857996

Suppliers and Price of 4,4-Dimethoxytetrahydropyran-3-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
4,4-dimethoxyoxan-3-one
100mg
$ 155.00

Sigma-Aldrich
4,4-Dimethoxytetrahydropyran-3-one Aldrich
1g
$ 1270.00

Matrix Scientific
4,4-Dimethoxytetrahydropyran-3-one 95%
1g
$ 1647.00

Matrix Scientific
4,4-Dimethoxytetrahydropyran-3-one 95%
500mg
$ 1036.00

Crysdot
4,4-Dimethoxydihydro-2H-pyran-3(4H)-one 95+%
5g
$ 945.00

Crysdot
4,4-Dimethoxydihydro-2H-pyran-3(4H)-one 95+%
1g
$ 315.00

Biosynth Carbosynth
4,4-Dimethoxytetrahydropyran-3-one
100 mg
$ 380.00

Biosynth Carbosynth
4,4-Dimethoxytetrahydropyran-3-one
50 mg
$ 237.50

Biosynth Carbosynth
4,4-Dimethoxytetrahydropyran-3-one
250 mg
$ 700.00

Biosynth Carbosynth
4,4-Dimethoxytetrahydropyran-3-one
1 g
$ 1480.00

Total 13 raw suppliers

Chemical Property of 4,4-Dimethoxytetrahydropyran-3-one

Chemical Property:

PSA：44.76000
LogP:-0.03510
XLogP3:-0.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:160.07355886
Heavy Atom Count:11
Complexity:151

Purity/Quality:

97% ^*data from raw suppliers

4,4-dimethoxyoxan-3-one ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xn
Statements: 22

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1(CCOCC1=O)OC

Technology Process of 4,4-Dimethoxytetrahydropyran-3-one

There total 4 articles about 4,4-Dimethoxytetrahydropyran-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 104681-92-7
4,4-dimethoxytetrahydro-2H-pyran-3-ol

: 693245-80-6
4,4-dimethoxy-5,6-dihydro-2H-pyran-3(4H)-one

Guidance literature:: With tetrapropylammonium perruthennate; 4 A molecular sieve; 4-methylmorpholine N-oxide; In dichloromethane; for 3h;

Reference yield: 66.0%

: 4732-69-8
Chloro-oxo-acetic acid

: 693245-80-6
4,4-dimethoxy-5,6-dihydro-2H-pyran-3(4H)-one

Guidance literature:: Chloro-oxo-acetic acid; With dimethyl sulfoxide; In dichloromethane; at 0 ℃; for 0.5h;

With triethylamine; In dichloromethane; at 20 ℃;

Reference yield:

: 29943-42-8,143562-54-3
Tetrahydro-4H-pyran-4-one

: 693245-80-6
4,4-dimethoxy-5,6-dihydro-2H-pyran-3(4H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide; iodine / 2.17 h / 5 °C

2: sodium bromate; acetic acid / ruthenium(III) trichloride hydrate / acetonitrile; water / 2 h / 30 °C

With sodium bromate; iodine; acetic acid; potassium hydroxide; ruthenium(III) trichloride hydrate; In water; acetonitrile;