5-Deoxy-5-(2,3,4,10-tetrahydro-7,8-dimethyl-2,4-dioxobenzo[g]pteridin-10-yl)-D-arabinitol

Base Information

Chemical Name:5-Deoxy-5-(2,3,4,10-tetrahydro-7,8-dimethyl-2,4-dioxobenzo[g]pteridin-10-yl)-D-arabinitol
CAS No.:53187-52-3
Molecular Formula:C₁₇H₂₀N₄O₆
Molecular Weight:376.369
Hs Code.:
Mol file:53187-52-3.mol

Synonyms:5-Deoxy-5-(2,3,4,10-tetrahydro-7,8-dimethyl-2,4-dioxobenzo[g]pteridin-10-yl)-D-arabinitol

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Chemical Property of 5-Deoxy-5-(2,3,4,10-tetrahydro-7,8-dimethyl-2,4-dioxobenzo[g]pteridin-10-yl)-D-arabinitol

Chemical Property:

Purity/Quality:

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Technology Process of 5-Deoxy-5-(2,3,4,10-tetrahydro-7,8-dimethyl-2,4-dioxobenzo[g]pteridin-10-yl)-D-arabinitol

There total 10 articles about 5-Deoxy-5-(2,3,4,10-tetrahydro-7,8-dimethyl-2,4-dioxobenzo[g]pteridin-10-yl)-D-arabinitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13345-95-4,78692-23-6
1,5-dihydro-riboflavin

: 1464-43-3,2897-21-4,26932-45-6,29621-88-3
seleno-L-cystine

: 3614-08-2,10236-58-5,18312-66-8,176300-66-6
L-selenocysteine

: 83-88-5,482-11-1,482-12-2,3687-62-5,5978-87-0,13123-37-0,33210-89-8,35919-91-6,53187-51-2,53187-52-3,135681-43-5,42880-33-1
riboflavin

Guidance literature:: In aq. phosphate buffer; at 25 ℃; for 6h; pH=7; pH-value; Equilibrium constant;
DOI:10.1002/kin.21430

Reference yield:

: 95-64-7
4-amino-o-xylene

: 83-88-5,482-11-1,482-12-2,3687-62-5,5978-87-0,13123-37-0,33210-89-8,35919-91-6,53187-51-2,53187-52-3,135681-43-5,42880-33-1
riboflavin

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium cyanoborohydride / methanol / 48 h / Reflux

2.1: hydrogenchloride / water / 0.17 h / 0 °C

2.2: 0.5 h / 0 °C

3.1: butan-1-ol; acetic acid / 5 h / Reflux

With hydrogenchloride; sodium cyanoborohydride; In methanol; water; acetic acid; butan-1-ol;
DOI:10.1021/acs.joc.6b00640

Reference yield:

: 50-69-1
D-ribose

: 83-88-5,482-11-1,482-12-2,3687-62-5,5978-87-0,13123-37-0,33210-89-8,35919-91-6,53187-51-2,53187-52-3,135681-43-5,42880-33-1
riboflavin

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium cyanoborohydride / methanol / 48 h / Reflux

2.1: hydrogenchloride / water / 0.17 h / 0 °C

2.2: 0.5 h / 0 °C

3.1: butan-1-ol; acetic acid / 5 h / Reflux

With hydrogenchloride; sodium cyanoborohydride; In methanol; water; acetic acid; butan-1-ol;
DOI:10.1021/acs.joc.6b00640