1-Deoxy-1-(6-phenylazo-3,4-xylidino)-D-ribitol

Base Information

Chemical Name:1-Deoxy-1-(6-phenylazo-3,4-xylidino)-D-ribitol
CAS No.:21037-26-3
Molecular Formula:C19H25N3O4
Molecular Weight:359.425
Hs Code.:
European Community (EC) Number:244-163-8
DSSTox Substance ID:DTXSID101189430
Nikkaji Number:J191.740D
Mol file:21037-26-3.mol

Synonyms:21037-26-3;1-Deoxy-1-(6-phenylazo-3,4-xylidino)-D-ribitol;(2R,3S,4S)-5-(4,5-dimethyl-2-phenyldiazenylanilino)pentane-1,2,3,4-tetrol;1-Deoxy-1-[4,5-dimethyl-2-(phenylazo)phenylamino]-D-ribitol;3,4-Xylyl-6-phenylazo-D-ribitylamine;SCHEMBL10351519;DTXSID101189430;EINECS 244-163-8;1-Deoxy-1-{[4,5-dimethyl-2-(phenyldiazenyl)phenyl]amino}pentitol;1-(d-Ribosylamino)-3,4-dimethylphenyl-6-azobenzene;W-109183;1-[2-(Phenylazo)-4,5-dimethylanilino]-1-deoxy-D-ribitol;1-Deoxy-1-[[4,5-dimethyl-2-(2-phenyldiazenyl)phenyl]amino]-D-ribito

Suppliers and Price of 1-Deoxy-1-(6-phenylazo-3,4-xylidino)-D-ribitol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
3,4-Xylyl-6-phenylazo-D-ribitylamine
1 g
$ 1055.00

TRC
3,4-Xylyl-6-phenylazo-D-ribitylamine
500 mg
$ 605.00

Total 12 raw suppliers

Chemical Property of 1-Deoxy-1-(6-phenylazo-3,4-xylidino)-D-ribitol

Chemical Property:

Vapor Pressure:1.08E-17mmHg at 25°C
Melting Point:>170?C (dec.)
Boiling Point:648.3°Cat760mmHg
Flash Point:345.9°C
PSA：117.67000
Density:1.27g/cm³
LogP:2.27870
Storage Temp.:-20°C Freezer, Under inert atmosphere
Solubility.:DMSO (Slightly), Ethyl Acetate, Methanol (Slightly)
XLogP3:2.4
Hydrogen Bond Donor Count:5
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:8
Exact Mass:359.18450629
Heavy Atom Count:26
Complexity:431

Purity/Quality:

98%min ^*data from raw suppliers

3,4-Xylyl-6-phenylazo-D-ribitylamine ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC(=C(C=C1C)N=NC2=CC=CC=C2)NCC(C(C(CO)O)O)O
Isomeric SMILES:CC1=CC(=C(C=C1C)N=NC2=CC=CC=C2)NC[C@@H]([C@@H]([C@@H](CO)O)O)O
Uses Riboflavin intermediate.

Technology Process of 1-Deoxy-1-(6-phenylazo-3,4-xylidino)-D-ribitol

There total 12 articles about 1-Deoxy-1-(6-phenylazo-3,4-xylidino)-D-ribitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 83916-71-6
N-ribityl-3,4-dimethylaniline

: 62-53-3
aniline

: 21037-26-3,113473-93-1
N-ribityl-2-phenylazo-4,5-dimethylaniline

Guidance literature:: aniline; With hydrogenchloride; In water; at 0 ℃; for 0.166667h;

With sodium nitrite; In water; at 0 ℃; for 0.5h;

N-ribityl-3,4-dimethylaniline; Further stages;
DOI:10.1021/acs.joc.6b00640