4-Aminotetrahydro-2H-pyran acetate

Base Information

• Chemical Name: 4-Aminotetrahydro-2H-pyran acetate
• CAS No.: 100549-89-1
• Molecular Formula: C₃₆H₃₂N₄O₅
• Molecular Weight: 600.674

Synonyms:4-Aminotetrahydro-2H-pyran acetate;Tetrahydro-2H-pyran-4-amine acetate;Tetrahydro-2H-pyran-4-amine acetate, 4-Aminooxane acetate;4-Aminotetrahydro-2H-pyranacetate98%

Chemical Property of 4-Aminotetrahydro-2H-pyran acetate

Chemical Property:

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

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MSDS Files:

SDS file from LookChem

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Technology Process of 4-Aminotetrahydro-2H-pyran acetate

There total 1 articles about 4-Aminotetrahydro-2H-pyran acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-chloroacetylamino-1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazole (3608-86-4) + Ethyl 3,3-diphenyl-2-oxoindoline-4-carboxylate (78034-08-9) → 3,3-Diphenyl-4-ethoxycarbonyl-2-oxoindoline-1-acet-4-antipyrylamide (100549-89-1)

Guidance literature:

With sodium ethanolate; Yield given. Multistep reaction; 1.) EtOH, toluene, 2.) reflux, 1.5 h;

DOI:10.1007/BF01148381

Reference yield: 38.0%

3,3-Diphenyl-4-ethoxycarbonyl-2-oxoindoline-1-acet-4-antipyrylamide (100549-89-1) → 3,3-Diphenyl-4-carboxy-2-oxoindoline-1-acet-4-antipyrylamide (100549-96-0)

Guidance literature:

With sodium hydroxide; In ethanol; for 0.5h; Heating;

DOI:10.1007/BF01148381

upstream raw materials:

4-chloroacetylamino-1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazole

Ethyl 3,3-diphenyl-2-oxoindoline-4-carboxylate

Downstream raw materials:

3,3-Diphenyl-4-carboxy-2-oxoindoline-1-acet-4-antipyrylamide

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