Methyl 3-(4-nitrophenyl)propionoate

Base Information

• Chemical Name: Methyl 3-(4-nitrophenyl)propionoate
• CAS No.: 54405-42-4
• Molecular Formula: C10H11NO4
• Molecular Weight: 209.202
• Hs Code.: 2916399090
• Mol file: 54405-42-4.mol

Synonyms:Methyl 3-(4-nitrophenyl)propionoate;methyl 3-(4-nitrophenyl)propanoate

Chemical Property of Methyl 3-(4-nitrophenyl)propionoate

Chemical Property:

• PSA: 72.12000
• LogP: 2.22360

Purity/Quality:

99% ^*data from raw suppliers

Methyl 3-(4-nitrophenyl)propionoate 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Methyl 3-(4-nitrophenyl)propionoate

There total 19 articles about Methyl 3-(4-nitrophenyl)propionoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

3-(4-nitrophenyl)propionic acid (16642-79-8) + diazomethyl-trimethyl-silane (18107-18-1) → methyl 3-(4-nitrophenyl)propanoate (54405-42-4)

Guidance literature:

With methanol; In hexane; at 0 ℃;

Reference yield: 86.0%

3-phenylpropanoic acid methyl ester (103-25-3) → methyl 3-(4-nitrophenyl)propanoate (54405-42-4)

Guidance literature:

With trifluoromethylsulfonic anhydride; tetrabutylammonium nitrate; In dichloromethane; at -30 ℃; for 1h; Inert atmosphere;

DOI:10.1021/acs.orglett.1c00868

Reference yield: 79.0%

C10H11N3O4 (1160845-77-1) → methyl 3-(4-nitrophenyl)propanoate (54405-42-4)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In chloroform; for 24h; Reflux;

DOI:10.1016/j.tetlet.2009.03.118

upstream raw materials:

1-phenoxy-1-isopropoxy-2-(4-nitrophenyl)cyclopropane

acrylic acid methyl ester

4-nitrophenylhydrazone

methanol

Downstream raw materials:

methyl 3-(4-aminophenyl)propionate

3-(4-amino-3-bromo-phenyl)-propionic acid methyl ester

3-(4-nitro-phenyl)-propionic acid hydrazide

methyl 3-(4-(methylsulfonamido)phenyl)propanoate

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