2-Chloro-3,4-diiodopyridine

Base Information

Chemical Name:2-Chloro-3,4-diiodopyridine
CAS No.:153034-91-4
Molecular Formula:C₅H₂ClI₂N
Molecular Weight:365.34
Hs Code.:
European Community (EC) Number:687-437-6
DSSTox Substance ID:DTXSID70439808
Nikkaji Number:J566.211G
Wikidata:Q82255891
Mol file:153034-91-4.mol

Synonyms:2-Chloro-3,4-diiodopyridine;153034-91-4;DTXSID70439808;BCP18313;MFCD16878974;2-Chloro-3,4-diiodopyridine, 97%;AS-59156;CS-0037697;W13637;A856593

Suppliers and Price of 2-Chloro-3,4-diiodopyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
2-Chloro-3,4-diiodopyridine 97%
500mg
$ 26.00

Chemenu
2-chloro-3,4-diiodopyridine 95%
1g
$ 422.00

AOBChem
2-Chloro-3,4-diiodopyridine 97%
500mg
$ 59.00

AOBChem
2-Chloro-3,4-diiodopyridine 97%
10g
$ 480.00

American Custom Chemicals Corporation
2-CHLORO-3,4-DIIODOPYRIDINE 95.00%
50MG
$ 119.70

American Custom Chemicals Corporation
2-CHLORO-3,4-DIIODOPYRIDINE 95.00%
500MG
$ 627.00

AK Scientific
2-chloro-3,4-diiodopyridine
250mg
$ 131.60

Activate Scientific
2-Chloro-3,4-diiodopyridine 95%
25 g
$ 1231.00

Total 9 raw suppliers

Chemical Property of 2-Chloro-3,4-diiodopyridine

Chemical Property:

Melting Point:159-163°C
Boiling Point:338.7±42.0 °C(Predicted)
PKA:-0.87±0.10(Predicted)
PSA：12.89000
Density:2.633±0.06 g/cm3(Predicted)
LogP:2.94420
Storage Temp.:under inert gas (nitrogen or Argon) at 2–8 °C
XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:364.79652
Heavy Atom Count:9
Complexity:101

Purity/Quality:

97% ^*data from raw suppliers

2-Chloro-3,4-diiodopyridine 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xn
Statements: 22-36/37/38
Safety Statements: 26

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CN=C(C(=C1I)I)Cl

Technology Process of 2-Chloro-3,4-diiodopyridine

There total 2 articles about 2-Chloro-3,4-diiodopyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 78607-36-0
2-chloro-3-iodopyridine

: 153034-91-4
2-chloro-3,4-diiodopyridine

Guidance literature:: With iodine; lithium diisopropyl amide; In tetrahydrofuran; 1.) -75 deg C, 3 h, 2.) -75 deg C, 2 h;
DOI:10.1021/jo00079a031

Reference yield: 28.0%

: 109-09-1
2-chloropyridine

: 153034-91-4
2-chloro-3,4-diiodopyridine

Guidance literature:: 2-chloropyridine; With n-hexyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -78 ℃; for 1.5h; Inert atmosphere;

With iodine; In tetrahydrofuran; hexane; at -78 - 0 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2009.11.066