1-[(3aS,8aS)-tetrahydro-2,2-diMethyl-4,4,8,8-tetraphenyl-1,3-dioxolo[4,5-e][1,3,2]dioxaphosphepin-6-yl]-Pyrrolidine

Base Information

Chemical Name:1-[(3aS,8aS)-tetrahydro-2,2-diMethyl-4,4,8,8-tetraphenyl-1,3-dioxolo[4,5-e][1,3,2]dioxaphosphepin-6-yl]-Pyrrolidine
CAS No.:582298-51-9
Molecular Formula:C₃₅H₃₆NO₄P
Molecular Weight:565.649
Hs Code.:
Mol file:582298-51-9.mol

Synonyms:1-[(3aS,8aS)-tetrahydro-2,2-diMethyl-4,4,8,8-tetraphenyl-1,3-dioxolo[4,5-e][1,3,2]dioxaphosphepin-6-yl]-Pyrrolidine

Suppliers and Price of 1-[(3aS,8aS)-tetrahydro-2,2-diMethyl-4,4,8,8-tetraphenyl-1,3-dioxolo[4,5-e][1,3,2]dioxaphosphepin-6-yl]-Pyrrolidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 9 raw suppliers

Chemical Property of 1-[(3aS,8aS)-tetrahydro-2,2-diMethyl-4,4,8,8-tetraphenyl-1,3-dioxolo[4,5-e][1,3,2]dioxaphosphepin-6-yl]-Pyrrolidine

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of 1-[(3aS,8aS)-tetrahydro-2,2-diMethyl-4,4,8,8-tetraphenyl-1,3-dioxolo[4,5-e][1,3,2]dioxaphosphepin-6-yl]-Pyrrolidine

There total 2 articles about 1-[(3aS,8aS)-tetrahydro-2,2-diMethyl-4,4,8,8-tetraphenyl-1,3-dioxolo[4,5-e][1,3,2]dioxaphosphepin-6-yl]-Pyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 123-75-1
pyrrolidine

: 299917-90-1
(3aR,8aR)-6-chloro-2,2-dimethyl-4,4,8,8-tetraphenyltetrahydro[1,3]dioxolo[4,5-e][1,3,2]dioxaphosphepine

: 582298-51-9,913706-72-6
1-((3aR,8aR)-2,2-dimethyl-4,4,8,8-tetraphenyltetrahydro-[1,3]dioxolo[4,5-e][1,3,2]dioxaphosphepine-6-yl)pyrrolidine

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; Molecular sieve; Inert atmosphere;
DOI:10.1002/chem.201500352

Reference yield: 42.0%

: 123-75-1
pyrrolidine

: 93379-48-7
(R,R)-TADDOL

: 582298-51-9,913706-72-6
1-((3aR,8aR)-2,2-dimethyl-4,4,8,8-tetraphenyltetrahydro-[1,3]dioxolo[4,5-e][1,3,2]dioxaphosphepine-6-yl)pyrrolidine

Guidance literature:: (R,R)-TADDOL; With 4 Angstroem MS; triethylamine; phosphorus trichloride; In tetrahydrofuran; at 20 ℃; for 0.666667h;

pyrrolidine; In tetrahydrofuran; at 20 ℃;
DOI:10.1021/ja064868m