3-(4-chlorophenyl)-2,3-dihydro-2-thioxo-Thieno[2,3-d]pyrimidin-4(1H)-one

Base Information

Chemical Name:3-(4-chlorophenyl)-2,3-dihydro-2-thioxo-Thieno[2,3-d]pyrimidin-4(1H)-one
CAS No.:468096-21-1
Molecular Formula:C₁₂H₇ClN₂OS₂
Molecular Weight:0
Hs Code.:
Mol file:468096-21-1.mol

Synonyms:3-(4-chlorophenyl)-2,3-dihydro-2-thioxo-Thieno[2,3-d]pyrimidin-4(1H)-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(4-chlorophenyl)-2,3-dihydro-2-thioxo-Thieno[2,3-d]pyrimidin-4(1H)-one

Chemical Property:

Purity/Quality:

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MSDS Files:: SDS file from LookChem

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Technology Process of 3-(4-chlorophenyl)-2,3-dihydro-2-thioxo-Thieno[2,3-d]pyrimidin-4(1H)-one

There total 3 articles about 3-(4-chlorophenyl)-2,3-dihydro-2-thioxo-Thieno[2,3-d]pyrimidin-4(1H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 468096-16-4
methyl 2-({[(4-chlorophenyl)amino]carbonothioyl}amino)thiophene-3-carboxylate

: 468096-21-1
3-(4-chlorophenyl)-2-mercaptothieno[2,3-d]pyrimidin-4(3H)-one

Guidance literature:: With potassium hydroxide; In water; for 1h; Heating;
DOI:10.1211/0022357021778871

Reference yield:

: 4651-81-4
Methyl 2-aminothiophene-3-carboxylate

: 468096-21-1
3-(4-chlorophenyl)-2-mercaptothieno[2,3-d]pyrimidin-4(3H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: 52 percent / ethanol / 2.5 h / Heating

2: 90 percent / KOH / H₂O / 1 h / Heating

With potassium hydroxide; In ethanol; water;
DOI:10.1211/0022357021778871

Reference yield:

: 2131-55-7
4-Chlorophenyl isothiocyanate

: 468096-21-1
3-(4-chlorophenyl)-2-mercaptothieno[2,3-d]pyrimidin-4(3H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: 52 percent / ethanol / 2.5 h / Heating

2: 90 percent / KOH / H₂O / 1 h / Heating

With potassium hydroxide; In ethanol; water;
DOI:10.1211/0022357021778871