Technology Process of L-MENTHYL-A-D-GLUCOPYRANOSIDE N-HYDRATE
There total 11 articles about L-MENTHYL-A-D-GLUCOPYRANOSIDE N-HYDRATE which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: Hepes buffer; Catharanthus roseus GTF-I glucosyltransferase / 36 h / 35 °C / pH 7.0 / Enzymatic reaction
2: almond-β-glucosidase; phosphate buffer / 24 h / 37 °C / pH 6.0 / Enzymatic reaction
3: 1,1,3,3-tetramethylguanidine; BF3*OEt2 / acetonitrile / 2 h / 20 °C
4: K2CO3 / H2O
With
phosphate buffer; almond-β-glucosidase; HEPES buffer; boron trifluoride diethyl etherate; potassium carbonate; N,N,N',N'-tetramethylguanidine; Catharanthus roseus GTF-I glucosyltransferase;
In
water; acetonitrile;
DOI:10.1016/j.tetasy.2004.06.022
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1,1,3,3-tetramethylguanidine; BF3*OEt2 / acetonitrile / 2 h / 20 °C
2: K2CO3 / H2O
With
boron trifluoride diethyl etherate; potassium carbonate; N,N,N',N'-tetramethylguanidine;
In
water; acetonitrile;
DOI:10.1016/j.tetasy.2004.06.022
- Guidance literature:
-
Multi-step reaction with 3 steps
1: almond-β-glucosidase; phosphate buffer / 24 h / 37 °C / pH 6.0 / Enzymatic reaction
2: 1,1,3,3-tetramethylguanidine; BF3*OEt2 / acetonitrile / 2 h / 20 °C
3: K2CO3 / H2O
With
phosphate buffer; almond-β-glucosidase; boron trifluoride diethyl etherate; potassium carbonate; N,N,N',N'-tetramethylguanidine;
In
water; acetonitrile;
DOI:10.1016/j.tetasy.2004.06.022