N-Boc-2-bromo-3-methylphenylamine

Base Information

Chemical Name:N-Boc-2-bromo-3-methylphenylamine
CAS No.:936829-27-5
Molecular Formula:C12H16BrNO2
Molecular Weight:286.169
Hs Code.:

Synonyms:(2-Bromo-3-methylphenyl)carbamic acid tert-butyl ester;N-Boc-2-bromo-3-methylaniline;N-Boc-2-bromo-3-methylphenylamine

Suppliers and Price of N-Boc-2-bromo-3-methylphenylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
N-Boc-2-bromo-3-methylaniline 97%
1g
$ 53.20

Chemcia Scientific
(2-Bromo-3-methyl-phenyl)-carbamicacidtert-butylester 95%
5 G
$ 995.00

Chemcia Scientific
(2-Bromo-3-methyl-phenyl)-carbamicacidtert-butylester 95%
1 G
$ 295.00

AK Scientific
N-Boc-2-bromo-3-methylaniline
1g
$ 133.00

Total 2 raw suppliers

Chemical Property of N-Boc-2-bromo-3-methylphenylamine

Chemical Property:

Melting Point:58-63°C
PSA：38.33000
LogP:4.17750

Purity/Quality:

99% ^*data from raw suppliers

N-Boc-2-bromo-3-methylaniline 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-Boc-2-bromo-3-methylphenylamine

There total 1 articles about N-Boc-2-bromo-3-methylphenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 14.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 54879-20-8
2-bromo-3-methylaniline

: 936829-27-5
tert-butyl 2-bromo-3-methylphenylcarbamate

Guidance literature:: With iodine; at 20 ℃; Inert atmosphere;
DOI:10.1021/jo802604g

Reference yield: 90.0%

: 936829-27-5
tert-butyl 2-bromo-3-methylphenylcarbamate

: 2917-46-6
bis(chloromethyl)dimethylsilane

: 1622406-52-3
tert-butyl 2-bromo-3-methylphenyl(((chloromethyl)dimethylsilyl)methyl)carbamate

Guidance literature:: tert-butyl 2-bromo-3-methylphenylcarbamate; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; for 0.0833333h; Inert atmosphere;

bis(chloromethyl)dimethylsilane; In N,N-dimethyl-formamide; mineral oil; at 80 ℃; Inert atmosphere;
DOI:10.1002/chem.201402597

Reference yield:

: 936829-27-5
tert-butyl 2-bromo-3-methylphenylcarbamate

: 73183-34-3
bis(pinacol)diborane

: 1186637-31-9
tert-butyl 3-methyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenylcarbamate

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium acetate; In 1,4-dioxane; at 100 ℃; Inert atmosphere;