5H-DIBENZO(b,e)(1,4)DIAZEPINE, 10,11-DIHYDRO-5,10-DIMETHYL-

Base Information

Chemical Name:5H-DIBENZO(b,e)(1,4)DIAZEPINE, 10,11-DIHYDRO-5,10-DIMETHYL-
CAS No.:32047-74-8
Molecular Formula:C₁₅H₁₆N₂
Molecular Weight:224.305
Hs Code.:
DSSTox Substance ID:DTXSID40185865
Nikkaji Number:J42.191J
Wikidata:Q83057005
Mol file:32047-74-8.mol

Synonyms:32047-74-8;5H-DIBENZO(b,e)(1,4)DIAZEPINE, 10,11-DIHYDRO-5,10-DIMETHYL-;5,10-Dimethyl-10,11-dihydro-5H-dibenzo(b,e)(1,4)diazepine;5H-Dibenzo[b,e][1,4]diazepine, 10,11-dihydro-5,10-dimethyl-;DTXSID40185865;LS-60891;5,11-Dimethyl-6H-benzo[c][1,5]benzodiazepine;10,11-Dihydro-5,10-dimethyl-5H-dibenzo[b,e][1,4]diazepine

Suppliers and Price of 5H-DIBENZO(b,e)(1,4)DIAZEPINE, 10,11-DIHYDRO-5,10-DIMETHYL-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 5H-DIBENZO(b,e)(1,4)DIAZEPINE, 10,11-DIHYDRO-5,10-DIMETHYL-

Chemical Property:

Vapor Pressure:1.72E-05mmHg at 25°C
Boiling Point:364.1°Cat760mmHg
Flash Point:162.6°C
PSA：6.48000
Density:1.089g/cm³
LogP:3.53430
XLogP3:3.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:224.131348519
Heavy Atom Count:17
Complexity:266

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1CC2=CC=CC=C2N(C3=CC=CC=C31)C

Technology Process of 5H-DIBENZO(b,e)(1,4)DIAZEPINE, 10,11-DIHYDRO-5,10-DIMETHYL-

There total 1 articles about 5H-DIBENZO(b,e)(1,4)DIAZEPINE, 10,11-DIHYDRO-5,10-DIMETHYL- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 3213-79-4
N,N'-dimethyl-1,2-phenylenediamine

: 3433-80-5
1-Bromo-2-bromomethyl-benzene

: 32047-74-8
5,10-dimethyl-10,11-dihydro-5H-dibenzo[b,e][1,4]diazepine

Guidance literature:: With palladium diacetate; potassium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In toluene; at 110 ℃; for 16h; chemoselective reaction; Inert atmosphere;
DOI:10.1002/ejoc.201402207