trans-1-(Perfluorophenyl)prop-1-ene, trans-1-(Pentafluorophenyl)prop-1-ene

Base Information

• Chemical Name: trans-1-(Perfluorophenyl)prop-1-ene, trans-1-(Pentafluorophenyl)prop-1-ene
• CAS No.: 4683-67-4
• Molecular Formula: C9H5F5
• Molecular Weight: 208.131
• Hs Code.: 2903998090
• Mol file: 4683-67-4.mol

Synonyms:1,2,3,4,5,-Pentafluoro-6-[(1E)-prop-1-en-1-yl]benzene;trans-1-(Perfluorophenyl)prop-1-ene, trans-1-(Pentafluorophenyl)prop-1-ene

Chemical Property of trans-1-(Perfluorophenyl)prop-1-ene, trans-1-(Pentafluorophenyl)prop-1-ene

Chemical Property:

• PSA: 0.00000
• LogP: 3.41520

Purity/Quality:

97% ^*data from raw suppliers

E-1-(Pentafluorophenyl)prop-1-ene 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of trans-1-(Perfluorophenyl)prop-1-ene, trans-1-(Pentafluorophenyl)prop-1-ene

There total 7 articles about trans-1-(Perfluorophenyl)prop-1-ene, trans-1-(Pentafluorophenyl)prop-1-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

1-allyl-2,3,4,5,6-pentafluorobenzene (1736-60-3) → (E)-1,2,3,4,5-pentafluoro-6-(prop-1-en-1-yl)benzene (4683-67-4)

Guidance literature:

With 4C₃H₉P*Ni*H⁽¹⁺⁾*C₂F₆NO₄S₂^(1-); In dichloromethane; Schlenk technique; Inert atmosphere;

DOI:10.1021/acs.joc.0c02033

Reference yield: 85.0%

1-allyl-2,3,4,5,6-pentafluorobenzene (1736-60-3) → 1,2,3,4,5-pentafluoro-6-(prop-1-en-1-yl)benzene (19140-58-0) + (E)-1,2,3,4,5-pentafluoro-6-(prop-1-en-1-yl)benzene (4683-67-4)

Guidance literature:

With manganese; 6,6'-dimethyl-2,2'-bipyridine; (1,2-dimethoxyethane)dichloronickel(II); phosphonic acid diethyl ester; In toluene; at 35 ℃; for 24h;

Reference yield:

1-allyl-2,3,4,5,6-pentafluorobenzene (1736-60-3) → 1,2,3,4,5-pentafluoro-6-(prop-1-en-1-yl)benzene (19140-58-0) + 1,2,3,4,5-pentafluoro-6-propylbenzene (52144-69-1) + (E)-1,2,3,4,5-pentafluoro-6-(prop-1-en-1-yl)benzene (4683-67-4)

Guidance literature:

With hydrido(phosphonite)cobalt(I); 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane; In dichloromethane; at 20 ℃; Overall yield = 58 percent; Overall yield = 24.3 mg; Schlenk technique; Inert atmosphere; Darkness;

DOI:10.1002/chem.202000410

upstream raw materials:

Hexafluorobenzene

(E)-propenyl lithium

2-Brom-1-pentafluorphenylpropan

bromopentafluorobenzene

Downstream raw materials:

1,2,4,5-Tetrafluor-3--6--benzol

1,2,4,5-tetrafluoro-3,6-bis[(E)-prop-1-en-1-yl]benzene

2,3,5,6-tetrafluoroterephthalic acid

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