2-CHLORO-4-METHOXY-6-NITRO TOLUENE

Base Information

Chemical Name:2-CHLORO-4-METHOXY-6-NITRO TOLUENE
CAS No.:102735-89-7
Molecular Formula:C8H8ClNO3
Molecular Weight:201.609
Hs Code.:
Mol file:102735-89-7.mol

Synonyms:2-CHLORO-4-METHOXY-6-NITRO TOLUENE

Suppliers and Price of 2-CHLORO-4-METHOXY-6-NITRO TOLUENE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-Chloro-4-methoxy-6-nitroToluene
10mg
$ 75.00

TRC
2-Chloro-4-methoxy-6-nitroToluene
2mg
$ 60.00

Crysdot
1-Chloro-5-methoxy-2-methyl-3-nitrobenzene 97%
250mg
$ 344.00

Crysdot
1-Chloro-5-methoxy-2-methyl-3-nitrobenzene 97%
1g
$ 860.00

American Custom Chemicals Corporation
2-CHLORO-4-METHOXY-6-NITRO TOLUENE 95.00%
5MG
$ 495.51

Alichem
3-Chloro-4-methyl-5-nitroanisole
1g
$ 1564.50

Alichem
3-Chloro-4-methyl-5-nitroanisole
500mg
$ 863.90

Alichem
3-Chloro-4-methyl-5-nitroanisole
250mg
$ 484.80

Total 4 raw suppliers

Chemical Property of 2-CHLORO-4-METHOXY-6-NITRO TOLUENE

Chemical Property:

Boiling Point:293.1±35.0 °C(Predicted)
PSA：55.05000
Density:1.313±0.06 g/cm3(Predicted)
LogP:3.08840

Purity/Quality:

97% ^*data from raw suppliers

2-Chloro-4-methoxy-6-nitroToluene ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-CHLORO-4-METHOXY-6-NITRO TOLUENE

There total 4 articles about 2-CHLORO-4-METHOXY-6-NITRO TOLUENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 16024-30-9
2-amino-4-methoxy-6-nitrotoluene

: 102735-89-7
2-chloro-4-methoxy-6-nitrotoluene

Guidance literature:: With hydrogenchloride; copper(l) chloride; sodium nitrite; In water; at 0 - 5 ℃; 2.) 10 min;
DOI:10.1021/ja00274a043

Reference yield:

: 446-10-6
2-nitro-4-fluorotoluene

: 102735-89-7
2-chloro-4-methoxy-6-nitrotoluene

Guidance literature:: Multi-step reaction with 4 steps

1: 45 percent / fuming nitric acid, fuming sulfuric acid / 6 h / 80 - 90 °C

2: 57 percent / sodium / 2 h / Heating

3: 35 percent / sodium bicarbonate, sodium sulfide nonahydrate / H₂O / 1 h / Heating

4: 58 percent / 1.) sodium nitrite, 12M HCl; 2.) copper(I) chloride / H₂O / 0 - 5 °C / 2.) 10 min

With hydrogenchloride; sodium sulfide; sulfuric acid; nitric acid; sodium; sodium hydrogencarbonate; copper(l) chloride; sodium nitrite; In water;
DOI:10.1021/ja00274a043

Reference yield:

: 16024-29-6
2,6-dinitro-4-methoxytoluene

: 102735-89-7
2-chloro-4-methoxy-6-nitrotoluene

Guidance literature:: Multi-step reaction with 2 steps

1: 35 percent / sodium bicarbonate, sodium sulfide nonahydrate / H₂O / 1 h / Heating

2: 58 percent / 1.) sodium nitrite, 12M HCl; 2.) copper(I) chloride / H₂O / 0 - 5 °C / 2.) 10 min

With hydrogenchloride; sodium sulfide; sodium hydrogencarbonate; copper(l) chloride; sodium nitrite; In water;
DOI:10.1021/ja00274a043