4'-METHOXY-4-BIPHENYLSULFONIC ACID

Base Information

Chemical Name:4'-METHOXY-4-BIPHENYLSULFONIC ACID
CAS No.:256439-82-4
Molecular Formula:C₁₃H₁₂O₄S
Molecular Weight:264.302
Hs Code.:
Mol file:256439-82-4.mol

Synonyms:4'-METHOXY-4-BIPHENYLSULFONIC ACID

Suppliers and Price of 4'-METHOXY-4-BIPHENYLSULFONIC ACID

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
4'-METHOXY-4-BIPHENYLSULFONIC ACID 95.00%
5MG
$ 499.88

Total 1 raw suppliers

Chemical Property of 4'-METHOXY-4-BIPHENYLSULFONIC ACID

Chemical Property:

PSA：71.98000
LogP:3.68970

Purity/Quality:: 4'-METHOXY-4-BIPHENYLSULFONIC ACID 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4'-METHOXY-4-BIPHENYLSULFONIC ACID

There total 2 articles about 4'-METHOXY-4-BIPHENYLSULFONIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 5720-07-0
4-methoxyphenylboronic acid

: 256439-82-4
4-(4-methoxyphenyl)-phenylsulfonic acid

Guidance literature:: 4-methoxyphenylboronic acid; 4-iodobenzenesulfonate-functionalized Argogel-MBOH resin; With potassium carbonate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In dichloromethane; N,N-dimethyl-formamide; Heating;

With trifluoroacetic acid; In dichloromethane; for 1h; Further stages.;
DOI:10.1021/ol991163z

Reference yield:

: 138-36-3
p-bromobenzene sulfonic acid

: 5720-07-0
4-methoxyphenylboronic acid

: 256439-82-4
4-(4-methoxyphenyl)-phenylsulfonic acid

Guidance literature:: With potassium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1,2-dimethoxyethane; water; at 80 ℃; for 3.5h;

Reference yield:

: 256439-82-4
4-(4-methoxyphenyl)-phenylsulfonic acid

: 202752-04-3
(4'-methoxy[1,1'-biphenyl]-4-yl)sulfonyl chloride

Guidance literature:: 4-(4-methoxyphenyl)-phenylsulfonic acid; With oxalyl dichloride; N,N-dimethyl-formamide; In tetrahydrofuran; at 0 - 20 ℃; for 18.5h;

With hydrogenchloride; In tetrahydrofuran; water;